2-Chloro-6-methylbenzo[D]oxazole

Base Information

Chemical Name:2-Chloro-6-methylbenzo[D]oxazole
CAS No.:3621-83-8
Molecular Formula:C₈H₆ClNO
Molecular Weight:167.595
Hs Code.:2934999090
DSSTox Substance ID:DTXSID40443336
Wikidata:Q82261090
Mol file:3621-83-8.mol

Synonyms:3621-83-8;2-CHLORO-6-METHYLBENZO[D]OXAZOLE;2-CHLORO-6-METHYL-1,3-BENZOXAZOLE;2-chloro-6-methyl-benzooxazole;2-CHLORO-6-METHYLBENZOXAZOLE;MFCD11890742;SCHEMBL2541637;DTXSID40443336;CLEOKTJHYLXEKQ-UHFFFAOYSA-N;AC6003;AKOS011655303;AB65043;FK-0712;SY130045;CS-0120827;EN300-97582;A913653

Suppliers and Price of 2-Chloro-6-methylbenzo[D]oxazole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

SynQuest Laboratories
2-Chloro-6-methyl-1,3-benzoxazole
1 g
$ 640.00

SynQuest Laboratories
2-Chloro-6-methyl-1,3-benzoxazole
500 mg
$ 472.00

Matrix Scientific
2-Chloro-6-methyl-1,3-benzoxazole >97%
1g
$ 730.00

Matrix Scientific
2-Chloro-6-methyl-1,3-benzoxazole >97%
500mg
$ 544.00

Alichem
2-Chloro-6-methylbenzo[d]oxazole
1g
$ 4563.02

Alichem
2-Chloro-6-methylbenzo[d]oxazole
500mg
$ 3303.49

AK Scientific
2-Chloro-6-methyl-1,3-benzoxazole
1g
$ 998.00

Total 8 raw suppliers

Chemical Property of 2-Chloro-6-methylbenzo[D]oxazole

Chemical Property:

Boiling Point:116-117 °C(Press: 10 Torr)
PKA:0.92±0.30(Predicted)
Density:1.311±0.06 g/cm3(Predicted)
XLogP3:3.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:167.0137915
Heavy Atom Count:11
Complexity:153

Purity/Quality:

99%, ^*data from raw suppliers

2-Chloro-6-methyl-1,3-benzoxazole ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC2=C(C=C1)N=C(O2)Cl

Technology Process of 2-Chloro-6-methylbenzo[D]oxazole

There total 3 articles about 2-Chloro-6-methylbenzo[D]oxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 23417-29-0
6-methylbenzo[d]oxazole-2-thiol

: 3621-83-8
2-chloro-6-methylbenzo[d]oxazole

Guidance literature:: With thionyl chloride; N,N-dimethyl-formamide; at 0 ℃; for 1h;

Reference yield:

: 2835-98-5
2-Hydroxy-4-methylanilin

: 3621-83-8
2-chloro-6-methylbenzo[d]oxazole

Guidance literature:: Multi-step reaction with 2 steps

1: KOH / ethanol / 8 h / Heating

2: PCl₅ / toluene / 1 h / 120 °C

With potassium hydroxide; phosphorus pentachloride; In ethanol; toluene;
DOI:10.1021/jm9801004