N-(2-{(1Z,4Z,9Z,15Z)-10,20-Bis-(2-amino-phenyl)-15-[2-(2,2-dimethyl-propionylamino)-phenyl]-porphyrin-5-yl}-phenyl)-2,2-dimethyl-propionamide

Base Information

• Chemical Name: N-(2-{(1Z,4Z,9Z,15Z)-10,20-Bis-(2-amino-phenyl)-15-[2-(2,2-dimethyl-propionylamino)-phenyl]-porphyrin-5-yl}-phenyl)-2,2-dimethyl-propionamide
• CAS No.: 90703-83-6
• Molecular Formula: C₅₄H₅₀N₈O₂
• Molecular Weight: 843.043

Synonyms:N-(2-{(1Z,4Z,9Z,15Z)-10,20-Bis-(2-amino-phenyl)-15-[2-(2,2-dimethyl-propionylamino)-phenyl]-porphyrin-5-yl}-phenyl)-2,2-dimethyl-propionamide

Chemical Property of N-(2-{(1Z,4Z,9Z,15Z)-10,20-Bis-(2-amino-phenyl)-15-[2-(2,2-dimethyl-propionylamino)-phenyl]-porphyrin-5-yl}-phenyl)-2,2-dimethyl-propionamide

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Technology Process of N-(2-{(1Z,4Z,9Z,15Z)-10,20-Bis-(2-amino-phenyl)-15-[2-(2,2-dimethyl-propionylamino)-phenyl]-porphyrin-5-yl}-phenyl)-2,2-dimethyl-propionamide

There total 4 articles about N-(2-{(1Z,4Z,9Z,15Z)-10,20-Bis-(2-amino-phenyl)-15-[2-(2,2-dimethyl-propionylamino)-phenyl]-porphyrin-5-yl}-phenyl)-2,2-dimethyl-propionamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tetrakis-5,10,15,20-(o-aminophenyl)porphyrin (52199-35-6) + pivaloyl chloride (3282-30-2) → (α,α,α,α)-5,10,15,20-tetrakisphenyl>-21H,23H-porphine (55253-62-8) + (α,α,α,α,)-5--phenyl>-10,15,20-tris(o-aminophenyl)-21H,23H-porphine (85294-19-5) + N-(2-{(1Z,4Z,9Z,15Z)-10,20-Bis-(2-amino-phenyl)-15-[2-(2,2-dimethyl-propionylamino)-phenyl]-porphyrin-5-yl}-phenyl)-2,2-dimethyl-propionamide (90703-83-6) + N-(2-{(5Z,10Z,14Z,19Z)-15,20-Bis-(2-amino-phenyl)-10-[2-(2,2-dimethyl-propionylamino)-phenyl]-porphyrin-5-yl}-phenyl)-2,2-dimethyl-propionamide (104070-02-2)

Guidance literature:

With pyridine; In dichloromethane; for 2h; Yield given. Further byproducts given;

DOI:10.1021/ja00282a020

Reference yield:

tetrakis-5,10,15,20-(o-aminophenyl)porphyrin (52199-35-6) + pivaloyl chloride (3282-30-2) → (α,α,α,α)-5,10,15,20-tetrakisphenyl>-21H,23H-porphine (55253-62-8) + meso-α-mono(o-aminophenyl)-α,α,α-tri(o-pivalamidophenyl)porphyrin (75557-89-0) + N-(2-{(1Z,4Z,9Z,15Z)-10,20-Bis-(2-amino-phenyl)-15-[2-(2,2-dimethyl-propionylamino)-phenyl]-porphyrin-5-yl}-phenyl)-2,2-dimethyl-propionamide (90703-83-6) + N-(2-{(5Z,10Z,14Z,19Z)-15,20-Bis-(2-amino-phenyl)-10-[2-(2,2-dimethyl-propionylamino)-phenyl]-porphyrin-5-yl}-phenyl)-2,2-dimethyl-propionamide (104070-02-2)

Guidance literature:

With pyridine; In dichloromethane; for 2h; Yield given. Further byproducts given. Title compound not separated from byproducts;

DOI:10.1021/ja00282a020

Reference yield:

pivaloyl chloride (3282-30-2) + 5,15-bis(α,α-o-aminophenyl)-10,20-bis<α,α-o-<(triphenylmethyl)amino>phenyl>porphyrin (104070-01-1) → N-(2-{(1Z,4Z,9Z,15Z)-10,20-Bis-(2-amino-phenyl)-15-[2-(2,2-dimethyl-propionylamino)-phenyl]-porphyrin-5-yl}-phenyl)-2,2-dimethyl-propionamide (90703-83-6)

Guidance literature:

With triethylamine; In dichloromethane;

DOI:10.1246/cl.2001.688

upstream raw materials:

tetrakis-5,10,15,20-(o-aminophenyl)porphyrin

pivaloyl chloride

5,15-bis(α,α-o-aminophenyl)-10,20-bis<α,α-o-<(triphenylmethyl)amino>phenyl>porphyrin

Downstream raw materials:

N-[2-((1Z,4Z,9Z,15Z)-15-[2-(2,2-Dimethyl-propionylamino)-phenyl]-10,20-bis-{2-[2-(2,5,6-trimethyl-benzoimidazol-1-yl)-acetylamino]-phenyl}-porphyrin-5-yl)-phenyl]-2,2-dimethyl-propionamide

α,α,5,15-bis-α,α,10,20-bis(pivalamidophenyl)porphine

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