Technology Process of (2-vinylhexyl)benzene
There total 4 articles about (2-vinylhexyl)benzene which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
benzyl bromide;
With
magnesium;
In
diethyl ether; ethylene dibromide;
at 20 ℃;
for 0.5h;
Inert atmosphere;
With
rhodium(III) chloride trihydrate; zinc(II) iodide;
In
diethyl ether;
at 20 ℃;
for 0.5h;
hept-1-en-3-yl (1,1,1,3,3,3-hexafluoropropan-2-yl) carbonate;
In
diethyl ether;
at 0 - 20 ℃;
for 16h;
DOI:10.1002/anie.202008071
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: dmap / dichloromethane / 24 h / 20 °C
2.1: magnesium / diethyl ether; ethylene dibromide / 0.5 h / 20 °C / Inert atmosphere
2.2: 0.5 h / 20 °C
2.3: 16 h / 0 - 20 °C
With
dmap; magnesium;
In
diethyl ether; dichloromethane; ethylene dibromide;
DOI:10.1002/anie.202008071
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: dichloromethane / 3 h / 20 °C / Inert atmosphere
2.1: dmap / dichloromethane / 24 h / 20 °C
3.1: magnesium / diethyl ether; ethylene dibromide / 0.5 h / 20 °C / Inert atmosphere
3.2: 0.5 h / 20 °C
3.3: 16 h / 0 - 20 °C
With
dmap; magnesium;
In
diethyl ether; dichloromethane; ethylene dibromide;
DOI:10.1002/anie.202008071