2-Acetyl-5-(2-carbomethoxy-6-methoxybenzoyloxy)-1,2,3,4-tetrahydronaphthalene

Base Information

Chemical Name:2-Acetyl-5-(2-carbomethoxy-6-methoxybenzoyloxy)-1,2,3,4-tetrahydronaphthalene
CAS No.:83344-25-6
Molecular Formula:C₂₂H₂₂O₆
Molecular Weight:382.413
Hs Code.:

Synonyms:2-Acetyl-5-(2-carbomethoxy-6-methoxybenzoyloxy)-1,2,3,4-tetrahydronaphthalene

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Chemical Property of 2-Acetyl-5-(2-carbomethoxy-6-methoxybenzoyloxy)-1,2,3,4-tetrahydronaphthalene

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Technology Process of 2-Acetyl-5-(2-carbomethoxy-6-methoxybenzoyloxy)-1,2,3,4-tetrahydronaphthalene

There total 5 articles about 2-Acetyl-5-(2-carbomethoxy-6-methoxybenzoyloxy)-1,2,3,4-tetrahydronaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 60314-07-0
2-methoxy-6-methoxycarbonylbenzoic acid

: 83344-23-4
2-Acetyl-5-hydroxy-1,2,3,4-tetrahydro naphthalene

: 83344-25-6
2-Acetyl-5-(2-carbomethoxy-6-methoxybenzoyloxy)-1,2,3,4-tetrahydronaphthalene

Guidance literature:: With trifluoroacetic anhydride; In dichloromethane; for 4h; Ambient temperature;

Reference yield: 80.0%

: 83344-23-4
2-Acetyl-5-hydroxy-1,2,3,4-tetrahydro naphthalene

: 60695-85-4
2-Carbomethoxy-6-methoxy-benzoyl chloride

: 83344-25-6
2-Acetyl-5-(2-carbomethoxy-6-methoxybenzoyloxy)-1,2,3,4-tetrahydronaphthalene

Guidance literature:: With pyridine; In benzene; for 6h; Ambient temperature;
DOI:10.1016/S0040-4039(00)87356-6

Reference yield:

: 83344-22-3
2-Acetyl-8-bromo-5-hydroxy-1,2,3,4-tetrahydronaphthalene-4-one

: 83344-25-6
2-Acetyl-5-(2-carbomethoxy-6-methoxybenzoyloxy)-1,2,3,4-tetrahydronaphthalene

Guidance literature:: Multi-step reaction with 2 steps

1: 45 percent / H₂ / PtO₂ / ethanol / 6 h / 760 Torr

2: 90 percent / (CF₃CO)2O / CH₂Cl₂ / 4 h / Ambient temperature

With hydrogen; trifluoroacetic anhydride; platinum(IV) oxide; In ethanol; dichloromethane;