1-[2-(2,6-diethyl-4-methylphenyl)-2-oxoacetyl]-1-methyl-2-[1-phenyl-1-ethylidene]hydrazine

Base Information

Chemical Name:1-[2-(2,6-diethyl-4-methylphenyl)-2-oxoacetyl]-1-methyl-2-[1-phenyl-1-ethylidene]hydrazine
CAS No.:1363808-99-4
Molecular Formula:C₂₂H₂₆N₂O₂
Molecular Weight:350.461
Hs Code.:

Synonyms:1-[2-(2,6-diethyl-4-methylphenyl)-2-oxoacetyl]-1-methyl-2-[1-phenyl-1-ethylidene]hydrazine

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Chemical Property of 1-[2-(2,6-diethyl-4-methylphenyl)-2-oxoacetyl]-1-methyl-2-[1-phenyl-1-ethylidene]hydrazine

Chemical Property:

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Technology Process of 1-[2-(2,6-diethyl-4-methylphenyl)-2-oxoacetyl]-1-methyl-2-[1-phenyl-1-ethylidene]hydrazine

There total 10 articles about 1-[2-(2,6-diethyl-4-methylphenyl)-2-oxoacetyl]-1-methyl-2-[1-phenyl-1-ethylidene]hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1363807-14-0
1-[2-(2,6-diethyl-4-methylphenyl)-2-oxoacetyl]-1-methylhydrazine

: 98-86-2
acetophenone

: 1363808-99-4
1-[2-(2,6-diethyl-4-methylphenyl)-2-oxoacetyl]-1-methyl-2-[1-phenyl-1-ethylidene]hydrazine

Guidance literature:: With acetic acid; In tetrahydrofuran; for 6h; Inert atmosphere; Reflux;

Reference yield:

: 314084-61-2
1-bromo-2,6-diethyl-4-methylbenzene

: 1363808-99-4
1-[2-(2,6-diethyl-4-methylphenyl)-2-oxoacetyl]-1-methyl-2-[1-phenyl-1-ethylidene]hydrazine

Guidance literature:: Multi-step reaction with 6 steps

1.1: magnesium; ethylene dibromide / toluene; tetrahydrofuran / 52 h / 40 - 50 °C / Inert atmosphere

1.2: 2 h / 0 - 5 °C / Inert atmosphere

2.1: hydrazine hydrate / methanol / 4.08 h / 1 - 2 °C

3.1: toluene / 2 h / 50 °C / 100 Torr / Inert atmosphere

4.1: potassium carbonate / toluene / 24 h / 5 °C

5.1: hydrogen / 5%-palladium/activated carbon / 1,2-dimethoxyethane / 8 h / 20 °C

6.1: acetic acid / tetrahydrofuran / 6 h / Inert atmosphere; Reflux

With hydrogen; potassium carbonate; hydrazine hydrate; magnesium; acetic acid; ethylene dibromide; 5%-palladium/activated carbon; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; toluene;

Reference yield:

: 1363806-98-7
ethyl 2-(2,6-diethyl-4-methylphenyl)-2-oxoacetate

: 1363808-99-4
1-[2-(2,6-diethyl-4-methylphenyl)-2-oxoacetyl]-1-methyl-2-[1-phenyl-1-ethylidene]hydrazine

Guidance literature:: Multi-step reaction with 5 steps

1: hydrazine hydrate / methanol / 4.08 h / 1 - 2 °C

2: methanol / 1.5 h / 20 °C

3: potassium carbonate / N,N-dimethyl-formamide / 2.5 h / 20 °C

4: hydroxylamine / water; methanol / 17 h / 50 - 60 °C

5: acetic acid / tetrahydrofuran / 6 h / Inert atmosphere; Reflux

With hydroxylamine; potassium carbonate; hydrazine hydrate; acetic acid; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;