(S)-1-(6-amino-9H-purin-9-yl)-4-(bis(4-methoxyphenyl)-(phenyl)methoxy)butan-2-ol

Base Information

Chemical Name:(S)-1-(6-amino-9H-purin-9-yl)-4-(bis(4-methoxyphenyl)-(phenyl)methoxy)butan-2-ol
CAS No.:1452390-87-2
Molecular Formula:C₃₀H₃₁N₅O₄
Molecular Weight:525.607
Hs Code.:

Synonyms:(S)-1-(6-amino-9H-purin-9-yl)-4-(bis(4-methoxyphenyl)-(phenyl)methoxy)butan-2-ol

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Chemical Property of (S)-1-(6-amino-9H-purin-9-yl)-4-(bis(4-methoxyphenyl)-(phenyl)methoxy)butan-2-ol

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Technology Process of (S)-1-(6-amino-9H-purin-9-yl)-4-(bis(4-methoxyphenyl)-(phenyl)methoxy)butan-2-ol

There total 1 articles about (S)-1-(6-amino-9H-purin-9-yl)-4-(bis(4-methoxyphenyl)-(phenyl)methoxy)butan-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 1452390-84-9
(S)-2-(2-(bis(4-methoxyphenyl)(phenyl)methoxy)ethyl)oxirane

: 66224-66-6,66224-67-7,66224-68-8,66224-69-9,134434-48-3,134434-49-4,134454-76-5,134461-75-9
adenine

: 1452390-87-2
(S)-1-(6-amino-9H-purin-9-yl)-4-(bis(4-methoxyphenyl)-(phenyl)methoxy)butan-2-ol

Guidance literature:: adenine; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 1h;

(S)-2-(2-(bis(4-methoxyphenyl)(phenyl)methoxy)ethyl)oxirane; In N,N-dimethyl-formamide; at 110 ℃; for 12h;
DOI:10.1039/c3ob41244j

Reference yield: 60.0%

: 1452390-87-2
(S)-1-(6-amino-9H-purin-9-yl)-4-(bis(4-methoxyphenyl)-(phenyl)methoxy)butan-2-ol

: 98-88-4
benzoyl chloride

: 1452390-88-3
(S)-N-(9-(4-(bis(4-methoxyphenyl)(phenyl)methoxy)-2-hydroxybutyl)-9H-purin-6-yl)benzamide

Guidance literature:: (S)-1-(6-amino-9H-purin-9-yl)-4-(bis(4-methoxyphenyl)-(phenyl)methoxy)butan-2-ol; With pyridine; chloro-trimethyl-silane; at 0 - 20 ℃; for 4.5h; Inert atmosphere;

benzoyl chloride; at 0 - 20 ℃; for 4h;
DOI:10.1039/c3ob41244j

Reference yield:

: 1452390-87-2
(S)-1-(6-amino-9H-purin-9-yl)-4-(bis(4-methoxyphenyl)-(phenyl)methoxy)butan-2-ol

: 1452390-98-5,1452390-99-6
C₄₆H₅₂N₇O₆P

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine; chloro-trimethyl-silane / 4.5 h / 0 - 20 °C / Inert atmosphere

1.2: 4 h / 0 - 20 °C

2.1: diisopropylammonium tetrazolide / dichloromethane / 0.02 h / Inert atmosphere

2.2: 3 h / 20 °C / Inert atmosphere

With pyridine; chloro-trimethyl-silane; diisopropylammonium tetrazolide; In dichloromethane;
DOI:10.1039/c3ob41244j