2-(2,6-Dichlorophenyl)-2,3-dihydroquinazolin-4(1h)-one

Base Information

• Chemical Name: 2-(2,6-Dichlorophenyl)-2,3-dihydroquinazolin-4(1h)-one
• CAS No.: 83800-94-6
• Molecular Formula: C14H10 Cl2 N2 O
• Molecular Weight: 293.152
• European Community (EC) Number: 653-696-9
• NSC Number: 158391
• ChEMBL ID: CHEMBL2000876

Synonyms:2-(2,6-dichlorophenyl)-2,3-dihydroquinazolin-4(1h)-one;83800-94-6;NSC158391;CHEMBL2000876;2-(2,6-DICHLOROPHENYL)-1,2-DIHYDRO-4(3H)-QUINAZOLINONE;AKOS001291356;AKOS016872588;NSC-158391;NCI60_001166;Z48978407;2-(2,6-dichlorophenyl)-1,2,3,4-tetrahydroquinazolin-4-one

Chemical Property of 2-(2,6-Dichlorophenyl)-2,3-dihydroquinazolin-4(1h)-one

Chemical Property:

• Vapor Pressure: 1.05E-10mmHg at 25°C
• Boiling Point: 514.8°Cat760mmHg
• Flash Point: 265.1°C
• Density: 1.376g/cm³
• XLogP3: 3.8
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 1
• Exact Mass: 292.0170183
• Heavy Atom Count: 19
• Complexity: 342

Purity/Quality:

98%,99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C2C(=C1)C(=O)NC(N2)C3=C(C=CC=C3Cl)Cl

Technology Process of 2-(2,6-Dichlorophenyl)-2,3-dihydroquinazolin-4(1h)-one

There total 2 articles about 2-(2,6-Dichlorophenyl)-2,3-dihydroquinazolin-4(1h)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

2,6-dichlorobenzaldehyde (83-38-5) + anthranilic acid amide (28144-70-9,88-68-6) → 2,3-dihydro-2-(2,6-dichlorophenyl)quinazolin-4(1H)-one (83800-94-6)

Guidance literature:

With BF₃-grafted Fe₃O₄(at)sucrose nanoparticles; at 20 ℃; for 0.25h;

DOI:10.1002/aoc.4431

Reference yield: 90.0%

isatoic anhydride (118-48-9) + 2,6-dichlorobenzaldehyde (83-38-5) → 2,3-dihydro-2-(2,6-dichlorophenyl)quinazolin-4(1H)-one (83800-94-6)

Guidance literature:

With ammonium acetate; for 0.666667h; Heating;

DOI:10.1007/s13738-016-1006-8

upstream raw materials:

2,6-dichlorobenzaldehyde

anthranilic acid amide

isatoic anhydride

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