(2S,3R,5R)-2-[6-(Trityl-amino)-purin-9-yl]-5-trityloxymethyl-tetrahydro-furan-3-ol

Base Information

Chemical Name:(2S,3R,5R)-2-[6-(Trityl-amino)-purin-9-yl]-5-trityloxymethyl-tetrahydro-furan-3-ol
CAS No.:216571-39-0
Molecular Formula:C₄₈H₄₁N₅O₃
Molecular Weight:735.885
Hs Code.:

Synonyms:(2S,3R,5R)-2-[6-(Trityl-amino)-purin-9-yl]-5-trityloxymethyl-tetrahydro-furan-3-ol

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Chemical Property of (2S,3R,5R)-2-[6-(Trityl-amino)-purin-9-yl]-5-trityloxymethyl-tetrahydro-furan-3-ol

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Technology Process of (2S,3R,5R)-2-[6-(Trityl-amino)-purin-9-yl]-5-trityloxymethyl-tetrahydro-furan-3-ol

There total 6 articles about (2S,3R,5R)-2-[6-(Trityl-amino)-purin-9-yl]-5-trityloxymethyl-tetrahydro-furan-3-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 170157-95-6
9-(3-deoxy-β-D-ribofuranosyl)adenine

: 216571-39-0
(2S,3R,5R)-2-[6-(Trityl-amino)-purin-9-yl]-5-trityloxymethyl-tetrahydro-furan-3-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 30 percent / pyridine

2: DEAD, PPh₃ / tetrahydrofuran

3: NH₃/CH₃OH

With pyridine; methanol; ammonia; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran;
DOI:10.1080/07328319808004708

Reference yield:

: 66224-66-6,66224-67-7,66224-68-8,66224-69-9,134434-48-3,134434-49-4,134454-76-5,134461-75-9
adenine

: 216571-39-0
(2S,3R,5R)-2-[6-(Trityl-amino)-purin-9-yl]-5-trityloxymethyl-tetrahydro-furan-3-ol

Guidance literature:: Multi-step reaction with 5 steps

1: 62 percent / SnCl₄ / acetonitrile / Ambient temperature

2: 80 percent / CH₃ONa / tetrahydrofuran

3: 30 percent / pyridine

4: DEAD, PPh₃ / tetrahydrofuran

5: NH₃/CH₃OH

With pyridine; methanol; ammonia; sodium methylate; tin(IV) chloride; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; acetonitrile;
DOI:10.1080/07328319808004708

Reference yield:

: 201287-86-7
Benzoic acid (2R,4S,5S)-4-acetoxy-5-(6-amino-purin-9-yl)-tetrahydro-furan-2-ylmethyl ester

: 216571-39-0
(2S,3R,5R)-2-[6-(Trityl-amino)-purin-9-yl]-5-trityloxymethyl-tetrahydro-furan-3-ol

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / CH₃ONa / tetrahydrofuran

2: 30 percent / pyridine

3: DEAD, PPh₃ / tetrahydrofuran

4: NH₃/CH₃OH

With pyridine; methanol; ammonia; sodium methylate; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran;
DOI:10.1080/07328319808004708