10,10-dimethyl-1,9,9-triphenyl-6-(prop-1-en-2-yl)-2,4,8-trioxa-9-silaundecan-6-ol

Base Information

Chemical Name:10,10-dimethyl-1,9,9-triphenyl-6-(prop-1-en-2-yl)-2,4,8-trioxa-9-silaundecan-6-ol
CAS No.:1429638-54-9
Molecular Formula:C₃₀H₃₈O₄Si
Molecular Weight:490.715
Hs Code.:

Synonyms:10,10-dimethyl-1,9,9-triphenyl-6-(prop-1-en-2-yl)-2,4,8-trioxa-9-silaundecan-6-ol

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Chemical Property of 10,10-dimethyl-1,9,9-triphenyl-6-(prop-1-en-2-yl)-2,4,8-trioxa-9-silaundecan-6-ol

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Technology Process of 10,10-dimethyl-1,9,9-triphenyl-6-(prop-1-en-2-yl)-2,4,8-trioxa-9-silaundecan-6-ol

There total 3 articles about 10,10-dimethyl-1,9,9-triphenyl-6-(prop-1-en-2-yl)-2,4,8-trioxa-9-silaundecan-6-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1429638-53-8
10,10-dimethyl-1,9,9-triphenyl-2,4,8-trioxa-9-silaundecan-6-one

: 13291-18-4
isopropenylmagnesium bromide

: 1429638-54-9
10,10-dimethyl-1,9,9-triphenyl-6-(prop-1-en-2-yl)-2,4,8-trioxa-9-silaundecan-6-ol

Guidance literature:: In tetrahydrofuran; at 0 - 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/ol4005799

Reference yield:

: 172843-09-3
1-O-(tert-butyldiphenylsilyl)-1,3-dihydroxy-2-propanone

: 1429638-54-9
10,10-dimethyl-1,9,9-triphenyl-6-(prop-1-en-2-yl)-2,4,8-trioxa-9-silaundecan-6-ol

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane / 24 h / 20 °C / Inert atmosphere

2: tetrahydrofuran / 0.5 h / 0 - 20 °C / Inert atmosphere

With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol4005799

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1429638-54-9
10,10-dimethyl-1,9,9-triphenyl-6-(prop-1-en-2-yl)-2,4,8-trioxa-9-silaundecan-6-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 18 h / 20 °C / Inert atmosphere

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 24 h / 20 °C / Inert atmosphere

3: tetrahydrofuran / 0.5 h / 0 - 20 °C / Inert atmosphere

With 1H-imidazole; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol4005799