[1-Methylsulfanyl-1-phenyl-meth-(Z)-ylidene]-thiophosphoramidic acid O,O'-diethyl ester

Base Information

Chemical Name:[1-Methylsulfanyl-1-phenyl-meth-(Z)-ylidene]-thiophosphoramidic acid O,O'-diethyl ester
CAS No.:125722-47-6
Molecular Formula:C₁₂H₁₈NO₂PS₂
Molecular Weight:303.386
Hs Code.:

Synonyms:[1-Methylsulfanyl-1-phenyl-meth-(Z)-ylidene]-thiophosphoramidic acid O,O'-diethyl ester

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Chemical Property of [1-Methylsulfanyl-1-phenyl-meth-(Z)-ylidene]-thiophosphoramidic acid O,O'-diethyl ester

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Technology Process of [1-Methylsulfanyl-1-phenyl-meth-(Z)-ylidene]-thiophosphoramidic acid O,O'-diethyl ester

There total 2 articles about [1-Methylsulfanyl-1-phenyl-meth-(Z)-ylidene]-thiophosphoramidic acid O,O'-diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 68206-76-8
N-(O,O-diethylthiophosphoryl)thiobenzamide

: 74-88-4
methyl iodide

: 125722-47-6
[1-Methylsulfanyl-1-phenyl-meth-(Z)-ylidene]-thiophosphoramidic acid O,O'-diethyl ester

Guidance literature:: With potassium hydroxide; In ethanol; for 4h; Ambient temperature;
DOI:10.1016/S0040-4020(01)89095-5

Reference yield:

: 100-47-0
benzonitrile

: 125722-47-6
[1-Methylsulfanyl-1-phenyl-meth-(Z)-ylidene]-thiophosphoramidic acid O,O'-diethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 58 percent / 2 h / 80 °C

2: 95 percent / KOH / ethanol / 4 h / Ambient temperature

With potassium hydroxide; In ethanol;
DOI:10.1016/S0040-4020(01)89095-5