C₈H₈INO

Base Information

Chemical Name:C₈H₈INO
CAS No.:1414860-51-7
Molecular Formula:C₈H₈INO
Molecular Weight:261.062
Hs Code.:

Synonyms:C₈H₈INO

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₈H₈INO

Chemical Property:

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Technology Process of C₈H₈INO

There total 3 articles about C₈H₈INO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1196977-45-3
5-oxo-3-cyclohexene-1-acetonitrile

: 1414860-51-7
C₈H₈INO

Guidance literature:: With pyridine; iodine; In chloroform; at 18 ℃;
DOI:10.1021/jo302132d

Reference yield:

: 930-68-7
cyclohexenone

: 1414860-51-7
C₈H₈INO

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / acetonitrile / 16 h / 18 °C

2: lithium chloride; water / dimethyl sulfoxide / 140 °C

3: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; toluene-4-sulfonic acid / dimethyl sulfoxide; toluene / 55 °C

4: iodine; pyridine / chloroform / 18 °C

With pyridine; water; iodine; potassium carbonate; toluene-4-sulfonic acid; lithium chloride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In chloroform; dimethyl sulfoxide; toluene; acetonitrile; 1: |Michael Addition;
DOI:10.1021/jo302132d

Reference yield:

: 86560-40-9
2-(3-oxocyclohexyl)acetonitrile

: 1414860-51-7
C₈H₈INO

Guidance literature:: Multi-step reaction with 2 steps

1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; toluene-4-sulfonic acid / dimethyl sulfoxide; toluene / 55 °C

2: iodine; pyridine / chloroform / 18 °C

With pyridine; iodine; toluene-4-sulfonic acid; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In chloroform; dimethyl sulfoxide; toluene;
DOI:10.1021/jo302132d