N,N-dimethyl-N'-<(2,2,2-trifluoroethylidene)amino>-1-cyclohexenecarboximidamide

Base Information

Chemical Name:N,N-dimethyl-N'-<(2,2,2-trifluoroethylidene)amino>-1-cyclohexenecarboximidamide
CAS No.:82691-80-3
Molecular Formula:C₁₁H₁₆F₃N₃
Molecular Weight:247.263
Hs Code.:

Synonyms:N,N-dimethyl-N'-<(2,2,2-trifluoroethylidene)amino>-1-cyclohexenecarboximidamide

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Chemical Property of N,N-dimethyl-N'-<(2,2,2-trifluoroethylidene)amino>-1-cyclohexenecarboximidamide

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Technology Process of N,N-dimethyl-N'-<(2,2,2-trifluoroethylidene)amino>-1-cyclohexenecarboximidamide

There total 3 articles about N,N-dimethyl-N'-<(2,2,2-trifluoroethylidene)amino>-1-cyclohexenecarboximidamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 82691-76-7
N-<(2,2,2-trifluoroethylidene)amino>-1-cyclohexenecarboximidoyl chloride

: 124-40-3
dimethyl amine

: 82691-80-3
N,N-dimethyl-N'-<(2,2,2-trifluoroethylidene)amino>-1-cyclohexenecarboximidamide

Guidance literature:: In diethyl ether; at 20 ℃; for 24h;
DOI:10.1021/jo00141a012

Reference yield:

: 80967-56-2,80967-61-9
4-chloro-2-(1-chloro-2,2,2-trifluoroethyl)-1-thia-2,3-diazaspiro<4.5>dec-3-ene 1-oxide

: 82691-80-3
N,N-dimethyl-N'-<(2,2,2-trifluoroethylidene)amino>-1-cyclohexenecarboximidamide

Guidance literature:: Multi-step reaction with 3 steps

1: 65 percent / 85percent m-chloroperbenzoic acid / CHCl₃ / 1.) a) 65-70 deg C, 1 h, b) RT, overnight

2: 71 percent / toluene / 2 h / Heating

3: 99 percent / diethyl ether / 24 h / 20 °C

With 3-chloro-benzenecarboperoxoic acid; In diethyl ether; chloroform; toluene;
DOI:10.1021/jo00141a012

Reference yield:

: 80967-59-5
4-chloro-2-(1-chloro-2,2,2-trifluoroethyl)-1-thia-2,3-diazaspiro<4.5>dec-3-ene 1,1-dioxide

: 82691-80-3
N,N-dimethyl-N'-<(2,2,2-trifluoroethylidene)amino>-1-cyclohexenecarboximidamide

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / toluene / 2 h / Heating

2: 99 percent / diethyl ether / 24 h / 20 °C

In diethyl ether; toluene;
DOI:10.1021/jo00141a012