5,5-diphenyl-1,9-bis(pentafluorobenzoyl)-dipyrromethane

Base Information

• Chemical Name: 5,5-diphenyl-1,9-bis(pentafluorobenzoyl)-dipyrromethane
• CAS No.: 1613337-25-9
• Molecular Formula: C₃₅H₁₆F₁₀N₂O₂
• Molecular Weight: 686.508
• Mol file: 1613337-25-9.mol

Synonyms:5,5-diphenyl-1,9-bis(pentafluorobenzoyl)-dipyrromethane

Chemical Property of 5,5-diphenyl-1,9-bis(pentafluorobenzoyl)-dipyrromethane

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 5,5-diphenyl-1,9-bis(pentafluorobenzoyl)-dipyrromethane

There total 3 articles about 5,5-diphenyl-1,9-bis(pentafluorobenzoyl)-dipyrromethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

pentafluorobenzoylchloride (2251-50-5) + diphenyldipyrrol-2-ylmethane (216683-34-0) → 5,5-diphenyl-1,9-bis(pentafluorobenzoyl)-dipyrromethane (1613337-25-9)

Guidance literature:

With phenylmagnesium bromide; In tetrahydrofuran;

DOI:10.1142/S1088424618500657

Reference yield: 32.0%

pentafluorobenzoylchloride (2251-50-5) + diphenyldipyrrol-2-ylmethane (216683-34-0) → 5,5-diphenyl-1,9-bis(pentafluorobenzoyl)-dipyrromethane (1613337-25-9) + C35H16F10N2O2

Guidance literature:

diphenyldipyrrol-2-ylmethane; With phenylmagnesium bromide; In tetrahydrofuran; at 20 ℃; for 0.166667h; Inert atmosphere;

pentafluorobenzoylchloride; In tetrahydrofuran; at 0 - 20 ℃; for 2h; Inert atmosphere;

DOI:10.1021/acs.orglett.6b03816

Reference yield:

benzophenone (119-61-9) → 5,5-diphenyl-1,9-bis(pentafluorobenzoyl)-dipyrromethane (1613337-25-9)

Guidance literature:

Multi-step reaction with 2 steps

1.1: boron trifluoride diethyl etherate / ethanol / 120 h / 20 °C / Inert atmosphere

2.1: ethylmagnesium bromide / toluene; tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

2.2: 0.5 h

With boron trifluoride diethyl etherate; ethylmagnesium bromide; In tetrahydrofuran; ethanol; toluene;

upstream raw materials:

pentafluorobenzoylchloride

diphenyldipyrrol-2-ylmethane

benzophenone

Downstream raw materials:

C₃₅H₂₀F₁₀N₂O₂