(-)-(3S,4R,5R)-3-(3',4',5'-trimethoxybenzyl)-4-<3'',4''-methylenedioxy-α,α-bis(phenylthio)benzyl>-5-(1-menthyloxy)butyrolactone

Base Information Edit

Chemical Name:(-)-(3S,4R,5R)-3-(3',4',5'-trimethoxybenzyl)-4-<3'',4''-methylenedioxy-α,α-bis(phenylthio)benzyl>-5-(1-menthyloxy)butyrolactone
CAS No.:140138-37-0
Molecular Formula:C₄₄H₅₀O₈S₂
Molecular Weight:771.008
Hs Code.:
Mol file:140138-37-0.mol

Synonyms:(-)-(3S,4R,5R)-3-(3',4',5'-trimethoxybenzyl)-4-<3'',4''-methylenedioxy-α,α-bis(phenylthio)benzyl>-5-(1-menthyloxy)butyrolactone

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Chemical Property of (-)-(3S,4R,5R)-3-(3',4',5'-trimethoxybenzyl)-4-<3'',4''-methylenedioxy-α,α-bis(phenylthio)benzyl>-5-(1-menthyloxy)butyrolactone Edit

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Technology Process of (-)-(3S,4R,5R)-3-(3',4',5'-trimethoxybenzyl)-4-<3'',4''-methylenedioxy-α,α-bis(phenylthio)benzyl>-5-(1-menthyloxy)butyrolactone

There total 2 articles about (-)-(3S,4R,5R)-3-(3',4',5'-trimethoxybenzyl)-4-<3'',4''-methylenedioxy-α,α-bis(phenylthio)benzyl>-5-(1-menthyloxy)butyrolactone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 21852-50-6
3,4,5-trimethoxybenzyl bromide

: 6302-93-8
5-[Bis(phenylsulfanyl)methyl]-1,3-benzodioxole

: 112968-75-9,122079-41-8,122079-45-2,135041-07-5,77934-87-3
(5R)-(L-menthyloxy)-2(5H)-furanone

: 140138-37-0
(-)-(3S,4R,5R)-3-(3',4',5'-trimethoxybenzyl)-4-<3'',4''-methylenedioxy-α,α-bis(phenylthio)benzyl>-5-(1-menthyloxy)butyrolactone

Guidance literature:: With n-butyllithium; desipramine; Yield given. Multistep reaction; 1) THF, hexane, -78 deg C, 3 h; 2) THF, hexane, -78 deg C, 2 h; 3) THF, hexane, -78 deg C --> room temperature, overnight;