(S)-4-Benzyl-3-[2-((R)-1-ethyl-2-methyl-allyloxy)-acetyl]-oxazolidin-2-one

Base Information

Chemical Name:(S)-4-Benzyl-3-[2-((R)-1-ethyl-2-methyl-allyloxy)-acetyl]-oxazolidin-2-one
CAS No.:406684-15-9
Molecular Formula:C₁₈H₂₃NO₄
Molecular Weight:317.385
Hs Code.:

Synonyms:(S)-4-Benzyl-3-[2-((R)-1-ethyl-2-methyl-allyloxy)-acetyl]-oxazolidin-2-one

Suppliers and Price of (S)-4-Benzyl-3-[2-((R)-1-ethyl-2-methyl-allyloxy)-acetyl]-oxazolidin-2-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-4-Benzyl-3-[2-((R)-1-ethyl-2-methyl-allyloxy)-acetyl]-oxazolidin-2-one

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Technology Process of (S)-4-Benzyl-3-[2-((R)-1-ethyl-2-methyl-allyloxy)-acetyl]-oxazolidin-2-one

There total 2 articles about (S)-4-Benzyl-3-[2-((R)-1-ethyl-2-methyl-allyloxy)-acetyl]-oxazolidin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 101711-90-4,123731-35-1,128677-61-2
(S)-4-benzyl-2-oxazolidinone lithium salt

: 406684-14-8
((R)-1-Ethyl-2-methyl-allyloxy)-acetic acid

: 406684-15-9
(S)-4-Benzyl-3-[2-((R)-1-ethyl-2-methyl-allyloxy)-acetyl]-oxazolidin-2-one

Guidance literature:: ((R)-1-Ethyl-2-methyl-allyloxy)-acetic acid; With tert-butylhypochlorite; triethylamine; In diethyl ether; at -78 - 0 ℃;

(S)-4-benzyl-2-oxazolidinone lithium salt; In tetrahydrofuran; diethyl ether; at -78 ℃; for 8h;
DOI:10.1002/1521-3773(20020104)41:1<176::AID-ANIE176>3.0.CO;2-#

Reference yield:

: 125637-07-2,2088-07-5
(R)-3-hydroxy-2-methylpent-1-ene

: 406684-15-9
(S)-4-Benzyl-3-[2-((R)-1-ethyl-2-methyl-allyloxy)-acetyl]-oxazolidin-2-one

Guidance literature:: Multi-step reaction with 2 steps

1.1: 100 percent / NaH / 8 h / 20 °C

2.1: (CH₃)3COCl; N(C₂H₅)3 / diethyl ether / -78 - 0 °C

2.2: 72 percent / tetrahydrofuran; diethyl ether / 8 h / -78 °C

With tert-butylhypochlorite; sodium hydride; triethylamine; In diethyl ether;
DOI:10.1002/1521-3773(20020104)41:1<176::AID-ANIE176>3.0.CO;2-#

Reference yield: 72.0%

: 556-56-9
allyl iodid

: 406684-15-9
(S)-4-Benzyl-3-[2-((R)-1-ethyl-2-methyl-allyloxy)-acetyl]-oxazolidin-2-one

: 406684-16-0
(S)-4-Benzyl-3-[(R)-2-((R)-1-ethyl-2-methyl-allyloxy)-pent-4-enoyl]-oxazolidin-2-one

Guidance literature:: With sodium hexamethyldisilazane; In tetrahydrofuran; at -78 - -45 ℃; for 5h;
DOI:10.1002/1521-3773(20020104)41:1<176::AID-ANIE176>3.0.CO;2-#