ZrCl(CH₂C(CH₃)3)3

Base Information

Chemical Name:ZrCl(CH₂C(CH₃)3)3
CAS No.:78097-75-3
Molecular Formula:C₁₅H₃₃ClZr
Molecular Weight:340.104
Hs Code.:

Synonyms:ZrCl(CH₂C(CH₃)3)3

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Chemical Property of ZrCl(CH₂C(CH₃)3)3

Chemical Property:

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Technology Process of ZrCl(CH₂C(CH₃)3)3

There total 3 articles about ZrCl(CH₂C(CH₃)3)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 10026-11-6
zirconium(IV) chloride

: 7412-67-1
neopentyl lithium

: 78097-75-3
ZrCl(CH₂C(CH₃)3)3

: Zr(neopentyl)4

Guidance literature:: In diethyl ether; byproducts: LiCl; inert atmosphere, absence of direct light; dropwise addn. of Li-compd. (in hexanes) to slight stoich. excess of ZrCl4 (in ether) at 0°C, stirring at room temp. overnight; filtration, solvent removal (vac.), sublimation (60°C); contg. tetraalkylcomplex as impurity;

Reference yield:

: 7412-67-1
neopentyl lithium

: 78097-75-3
ZrCl(CH₂C(CH₃)3)3

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether

2: diethyl ether

In diethyl ether;

Reference yield:

: 78068-02-7
Zr(CH₂C(CH₃)3)2Cl₂(CH₃CH₂OCH₂CH₃)2

: 19978-31-5
bis(neopentyl)magnesium

: 78097-75-3
ZrCl(CH₂C(CH₃)3)3

: 38010-72-9
tetraneopentyl zirconium

Guidance literature:: In diethyl ether; soln. of Mg compd. added to soln. of Zr complex at -78 °C, stirred for 2 h, under N2; evapd. in vac., sublimed for 10 h at 60 °C, identified by NMR;
DOI:10.1016/S0022-328X(00)82434-1