7-benzyloxy-3,4-dihydro(2H)-naphthalen-1-one-O-[(4-methylphenyl)sulfonyl]oxime

Base Information

Chemical Name:7-benzyloxy-3,4-dihydro(2H)-naphthalen-1-one-O-[(4-methylphenyl)sulfonyl]oxime
CAS No.:116906-99-1
Molecular Formula:C₂₄H₂₃NO₄S
Molecular Weight:421.517
Hs Code.:

Synonyms:7-benzyloxy-3,4-dihydro(2H)-naphthalen-1-one-O-[(4-methylphenyl)sulfonyl]oxime

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 7-benzyloxy-3,4-dihydro(2H)-naphthalen-1-one-O-[(4-methylphenyl)sulfonyl]oxime

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Technology Process of 7-benzyloxy-3,4-dihydro(2H)-naphthalen-1-one-O-[(4-methylphenyl)sulfonyl]oxime

There total 5 articles about 7-benzyloxy-3,4-dihydro(2H)-naphthalen-1-one-O-[(4-methylphenyl)sulfonyl]oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 116885-91-7
7-benzyloxy-3,4-dihydro-2H-naphthalen-1-one oxime

: 98-59-9
p-toluenesulfonyl chloride

: 116906-99-1
7-benzyloxy-3,4-dihydro(2H)-naphthalen-1-one-O-[(4-methylphenyl)sulfonyl]oxime

Guidance literature:: With pyridine; at 20 ℃; for 16h;
DOI:10.1016/j.tetlet.2013.11.113

Reference yield:

: 22009-38-7
7-hydroxy-1-tetralone

: 116906-99-1
7-benzyloxy-3,4-dihydro(2H)-naphthalen-1-one-O-[(4-methylphenyl)sulfonyl]oxime

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / potassium carbonate / dimethylformamide / 4 h / 80 - 100 °C

2: 89 percent / NH₂OH*HCl, pyridine / 12 h / Heating

3: 85 percent / pyridine / 16 h / Ambient temperature

With pyridine; hydroxylamine hydrochloride; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1139/v88-088

Reference yield:

: 32263-64-2
7-(benzyloxy)-3,4-dihydronaphthalen-1(2H)-one

: 116906-99-1
7-benzyloxy-3,4-dihydro(2H)-naphthalen-1-one-O-[(4-methylphenyl)sulfonyl]oxime

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / NH₂OH*HCl, pyridine / 12 h / Heating

2: 85 percent / pyridine / 16 h / Ambient temperature

With pyridine; hydroxylamine hydrochloride;
DOI:10.1139/v88-088