octaethyl cyclohexane-1,3-diylbis[methylene(aminomethylidenebisphosphonate)]

Base Information

Chemical Name:octaethyl cyclohexane-1,3-diylbis[methylene(aminomethylidenebisphosphonate)]
CAS No.:1620164-69-3
Molecular Formula:C₂₆H₅₈N₂O₁₂P₄
Molecular Weight:714.648
Hs Code.:

Synonyms:octaethyl cyclohexane-1,3-diylbis[methylene(aminomethylidenebisphosphonate)]

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Chemical Property of octaethyl cyclohexane-1,3-diylbis[methylene(aminomethylidenebisphosphonate)]

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Technology Process of octaethyl cyclohexane-1,3-diylbis[methylene(aminomethylidenebisphosphonate)]

There total 3 articles about octaethyl cyclohexane-1,3-diylbis[methylene(aminomethylidenebisphosphonate)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1620164-63-7
1,3-bis(isocyanomethyl)cyclohexane

: 122-52-1
triethyl phosphite

: 1620164-69-3
octaethyl cyclohexane-1,3-diylbis[methylene(aminomethylidenebisphosphonate)]

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; dichloromethane; at -15 ℃; for 1h;
DOI:10.1016/j.bmcl.2014.05.071

Reference yield:

: 2579-20-6
cis, trans-1,3-dimethylaminocyclohexane

: 1620164-69-3
octaethyl cyclohexane-1,3-diylbis[methylene(aminomethylidenebisphosphonate)]

Guidance literature:: Multi-step reaction with 3 steps

1.1: toluene / 8 h / Reflux

2.1: triethylamine / dichloromethane / 0 °C

2.2: 3 h / 0 - 20 °C

3.1: hydrogenchloride / dichloromethane; 1,4-dioxane / 1 h / -15 °C

With hydrogenchloride; triethylamine; In 1,4-dioxane; dichloromethane; toluene;
DOI:10.1016/j.bmcl.2014.05.071

Reference yield:

: 136869-17-5
C₁₀H₁₈N₂O₂

: 1620164-69-3
octaethyl cyclohexane-1,3-diylbis[methylene(aminomethylidenebisphosphonate)]

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / dichloromethane / 0 °C

1.2: 3 h / 0 - 20 °C

2.1: hydrogenchloride / dichloromethane; 1,4-dioxane / 1 h / -15 °C

With hydrogenchloride; triethylamine; In 1,4-dioxane; dichloromethane;
DOI:10.1016/j.bmcl.2014.05.071