cyclohexane-1,3-diylbis[methylene(aminomethylidenebisphosphonic)] acid

Base Information

Chemical Name:cyclohexane-1,3-diylbis[methylene(aminomethylidenebisphosphonic)] acid
CAS No.:1620164-76-2
Molecular Formula:C₁₀H₂₆N₂O₁₂P₄
Molecular Weight:490.218
Hs Code.:

Synonyms:cyclohexane-1,3-diylbis[methylene(aminomethylidenebisphosphonic)] acid

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Chemical Property of cyclohexane-1,3-diylbis[methylene(aminomethylidenebisphosphonic)] acid

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Technology Process of cyclohexane-1,3-diylbis[methylene(aminomethylidenebisphosphonic)] acid

There total 4 articles about cyclohexane-1,3-diylbis[methylene(aminomethylidenebisphosphonic)] acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1620164-69-3
octaethyl cyclohexane-1,3-diylbis[methylene(aminomethylidenebisphosphonate)]

: 1620164-76-2
cyclohexane-1,3-diylbis[methylene(aminomethylidenebisphosphonic)] acid

Guidance literature:: With hydrogenchloride; water; for 8h; Reflux;
DOI:10.1016/j.bmcl.2014.05.071

Reference yield:

: 2579-20-6
cis, trans-1,3-dimethylaminocyclohexane

: 1620164-76-2
cyclohexane-1,3-diylbis[methylene(aminomethylidenebisphosphonic)] acid

Guidance literature:: Multi-step reaction with 4 steps

1.1: toluene / 8 h / Reflux

2.1: triethylamine / dichloromethane / 0 °C

2.2: 3 h / 0 - 20 °C

3.1: hydrogenchloride / dichloromethane; 1,4-dioxane / 1 h / -15 °C

4.1: hydrogenchloride; water / 8 h / Reflux

With hydrogenchloride; water; triethylamine; In 1,4-dioxane; dichloromethane; toluene;
DOI:10.1016/j.bmcl.2014.05.071

Reference yield:

: 1620164-63-7
1,3-bis(isocyanomethyl)cyclohexane

: 1620164-76-2
cyclohexane-1,3-diylbis[methylene(aminomethylidenebisphosphonic)] acid

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / dichloromethane; 1,4-dioxane / 1 h / -15 °C

2: hydrogenchloride; water / 8 h / Reflux

With hydrogenchloride; water; In 1,4-dioxane; dichloromethane;
DOI:10.1016/j.bmcl.2014.05.071