2,6-dimethyl-5-carbomethoxy-4-(3'-nitrophenyl)-3-[3-(4'-methoxyphenyl)propane-1-one]-1,4-dihydropyridine

Base Information

• Chemical Name: 2,6-dimethyl-5-carbomethoxy-4-(3'-nitrophenyl)-3-[3-(4'-methoxyphenyl)propane-1-one]-1,4-dihydropyridine
• CAS No.: 366496-00-6
• Molecular Formula: C₂₅H₂₄N₂O₆
• Molecular Weight: 448.475

Synonyms:2,6-dimethyl-5-carbomethoxy-4-(3'-nitrophenyl)-3-[3-(4'-methoxyphenyl)propane-1-one]-1,4-dihydropyridine

Chemical Property of 2,6-dimethyl-5-carbomethoxy-4-(3'-nitrophenyl)-3-[3-(4'-methoxyphenyl)propane-1-one]-1,4-dihydropyridine

Chemical Property:

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Technology Process of 2,6-dimethyl-5-carbomethoxy-4-(3'-nitrophenyl)-3-[3-(4'-methoxyphenyl)propane-1-one]-1,4-dihydropyridine

There total 1 articles about 2,6-dimethyl-5-carbomethoxy-4-(3'-nitrophenyl)-3-[3-(4'-methoxyphenyl)propane-1-one]-1,4-dihydropyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

4-methoxy-benzaldehyde (123-11-5) + 4-(3'-nitrophenyl)-2,6-dimethyl-3-aceto-1,4-dihydropyridine-5-carboxylic acid methyl ester (89541-34-4) → 2,6-dimethyl-5-carbomethoxy-4-(3'-nitrophenyl)-3-[3-(4'-methoxyphenyl)propane-1-one]-1,4-dihydropyridine (366496-00-6)

Guidance literature:

With sodium hydroxide; In ethanol; at 25 - 30 ℃; for 24h; pH=8.0;

DOI:10.1515/HC.2001.7.2.167 DOI:10.1515/HC.2001.7.5.481

Reference yield: 62.0%

2,6-dimethyl-5-carbomethoxy-4-(3'-nitrophenyl)-3-[3-(4'-methoxyphenyl)propane-1-one]-1,4-dihydropyridine (366496-00-6) → 2,6-dimethyl-5-carbomethoxy-4-(3'-nitrophenyl)-3-[3-(4'-methoxyphenyl)-2H-pyrazoline-5'-yl]-1,4-dihydropyridine

Guidance literature:

With piperidine; hydrazine hydrate; In ethanol; for 10h; Heating;

DOI:10.1515/HC.2001.7.2.167

Reference yield: 58.0%

acetic acid (64-19-7,77671-22-8) + 2,6-dimethyl-5-carbomethoxy-4-(3'-nitrophenyl)-3-[3-(4'-methoxyphenyl)propane-1-one]-1,4-dihydropyridine (366496-00-6) → 2,6-dimethyl-5-carbomethoxy-4-(3'-nitrophenyl)-3-[3'-(4-methoxyphenyl)-2'-acetylpyrazoline-5'-yl]-1,4-dihydropyridine

Guidance literature:

With hydrazine hydrate; for 8h; Heating;

DOI:10.1515/HC.2001.7.2.167

upstream raw materials:

4-methoxy-benzaldehyde

4-(3'-nitrophenyl)-2,6-dimethyl-3-aceto-1,4-dihydropyridine-5-carboxylic acid methyl ester

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