C₆₀H₅₅Cl₂N₇O₁₆P₂

Base Information

• Chemical Name: C₆₀H₅₅Cl₂N₇O₁₆P₂
• CAS No.: 85240-02-4
• Molecular Formula: C₆₀H₅₅Cl₂N₇O₁₆P₂
• Molecular Weight: 1262.99
• Mol file: 85240-02-4.mol

Synonyms:C₆₀H₅₅Cl₂N₇O₁₆P₂

Chemical Property of C₆₀H₅₅Cl₂N₇O₁₆P₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₆₀H₅₅Cl₂N₇O₁₆P₂

There total 18 articles about C₆₀H₅₅Cl₂N₇O₁₆P₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-chlorophenyl phosphordi(1H-1-[1,2,4]triazolide) (72351-28-1) → C60H55Cl2N7O16P2 (85240-02-4)

Guidance literature:

Multi-step reaction with 5 steps

1: dioxane / 2 h / 20 °C

2: 1-methylimidazole / dioxane / 3 h / 20 °C

3: benzenesulfonic acid / CHCl₃; methanol / 0.25 h / 0 °C

4: 62 percent / 1-(2,4,6-triisopropylbenzenesulfonyl)-3-nitro-1,2,4-triazole / pyridine / 3.5 h / 20 °C

5: triethylamine / pyridine / 3 h / 20 °C

With 1-(2,4,6-triisopropylbenzenesulfonyl)-3-nitro-1,2,4-triazole; triethylamine; benzenesulfonic acid; 1-methyl-1H-imidazole; In 1,4-dioxane; pyridine; methanol; chloroform;

DOI:10.1002/hlca.19820650803

Reference yield:

2-chlorophenyl dichlorophosphate (15074-54-1) → C60H55Cl2N7O16P2 (85240-02-4)

Guidance literature:

Multi-step reaction with 6 steps

1: triethylamine / dioxane / 1 h / 20 °C

2: dioxane / 2 h / 20 °C

3: 1-methylimidazole / dioxane / 3 h / 20 °C

4: benzenesulfonic acid / CHCl₃; methanol / 0.25 h / 0 °C

5: 62 percent / 1-(2,4,6-triisopropylbenzenesulfonyl)-3-nitro-1,2,4-triazole / pyridine / 3.5 h / 20 °C

6: triethylamine / pyridine / 3 h / 20 °C

With 1-(2,4,6-triisopropylbenzenesulfonyl)-3-nitro-1,2,4-triazole; triethylamine; benzenesulfonic acid; 1-methyl-1H-imidazole; In 1,4-dioxane; pyridine; methanol; chloroform;

DOI:10.1002/hlca.19820650803

Reference yield:

C63H58Cl2N8O16P2 (78098-91-6) → C60H55Cl2N7O16P2 (85240-02-4)

Guidance literature:

With triethylamine; In pyridine; at 20 ℃; for 3h;

DOI:10.1002/hlca.19820650803

upstream raw materials:

C₆₃H₅₈Cl₂N₈O₁₆P₂

C₅₄H₅₁ClN₇O₁₃P

2-chlorophenyl dichlorophosphate

4,4'-dimethoxytrityl chloride