C₂₂H₂₅NO₆S

Base Information

Chemical Name:C₂₂H₂₅NO₆S
CAS No.:1446655-40-8
Molecular Formula:C₂₂H₂₅NO₆S
Molecular Weight:431.51
Hs Code.:

C<sub>22</sub>H<sub>25</sub>NO<sub>6</sub>S

Synonyms:C₂₂H₂₅NO₆S

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Chemical Property of C₂₂H₂₅NO₆S

Chemical Property:

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Technology Process of C₂₂H₂₅NO₆S

There total 10 articles about C₂₂H₂₅NO₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1446655-22-6
C₂₁H₂₃NO₄

: 124-63-0
methanesulfonyl chloride

: 1446655-40-8
C₂₂H₂₅NO₆S

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 0.5h;

Reference yield:

: 51-35-4,30724-02-8
4R-4-hydroxyproline

: 1446655-40-8
C₂₂H₂₅NO₆S

Guidance literature:: Multi-step reaction with 10 steps

1.1: thionyl chloride / Reflux

2.1: potassium carbonate / water; diethyl ether / 2 h / 0 - 20 °C

3.1: triethylamine / dichloromethane / 20 - 40 °C

4.1: cesium fluoride / N,N-dimethyl-formamide / 40 h / 60 °C

5.1: 1 h / 0 - 20 °C

5.2: 48 h / 20 °C

6.1: sodium hydroxide / tetrahydrofuran / 1.5 h / 0 - 20 °C

6.2: pH 3 - 4

7.1: borane-THF / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

8.1: palladium 10% on activated carbon; hydrogen / methanol / 760.05 Torr

9.1: potassium hydrogencarbonate / 0.5 h / 0 °C

10.1: triethylamine / dichloromethane / 0.5 h / 0 °C

With thionyl chloride; borane-THF; palladium 10% on activated carbon; hydrogen; potassium carbonate; potassium hydrogencarbonate; triethylamine; cesium fluoride; sodium hydroxide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 33996-30-4
trans-4-hydroxy-L-proline ethyl ester hydrochloride

: 1446655-40-8
C₂₂H₂₅NO₆S

Guidance literature:: Multi-step reaction with 9 steps

1.1: potassium carbonate / water; diethyl ether / 2 h / 0 - 20 °C

2.1: triethylamine / dichloromethane / 20 - 40 °C

3.1: cesium fluoride / N,N-dimethyl-formamide / 40 h / 60 °C

4.1: 1 h / 0 - 20 °C

4.2: 48 h / 20 °C

5.1: sodium hydroxide / tetrahydrofuran / 1.5 h / 0 - 20 °C

5.2: pH 3 - 4

6.1: borane-THF / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

7.1: palladium 10% on activated carbon; hydrogen / methanol / 760.05 Torr

8.1: potassium hydrogencarbonate / 0.5 h / 0 °C

9.1: triethylamine / dichloromethane / 0.5 h / 0 °C

With borane-THF; palladium 10% on activated carbon; hydrogen; potassium carbonate; potassium hydrogencarbonate; triethylamine; cesium fluoride; sodium hydroxide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide;