C₁₇H₂₂F₃N₅O₂S

Base Information

Chemical Name:C₁₇H₂₂F₃N₅O₂S
CAS No.:1223498-81-4
Molecular Formula:C₁₇H₂₂F₃N₅O₂S
Molecular Weight:417.455
Hs Code.:

C<sub>17</sub>H<sub>22</sub>F<sub>3</sub>N<sub>5</sub>O<sub>2</sub>S

Synonyms:C₁₇H₂₂F₃N₅O₂S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₇H₂₂F₃N₅O₂S

Chemical Property:

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Technology Process of C₁₇H₂₂F₃N₅O₂S

There total 7 articles about C₁₇H₂₂F₃N₅O₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₉H₂₁F₆N₅O₃S

: 1223498-81-4
C₁₇H₂₂F₃N₅O₂S

: 1223498-78-9
C₁₇H₂₂F₃N₅O₂S

Guidance literature:: With potassium carbonate; In methanol; at 20 ℃; for 1h;

Reference yield:

: 7205-60-9
1-(ethylsulfanyl)-4-nitrobenzene

: 1223498-81-4
C₁₇H₂₂F₃N₅O₂S

: 1223498-78-9
C₁₇H₂₂F₃N₅O₂S

Guidance literature:: Multi-step reaction with 6 steps

1: periodic acid / iron(III) chloride / acetonitrile / 0.83 h / 20 - 30 °C

2: sodium azide; sulfur trioxide; sulfuric acid / 6 h / 45 °C / cooling with ice; Inert atmosphere

3: triethylamine / dichloromethane / 3 h / 10 °C / cooling with ice

4: hydrogenchloride; titanium(III) chloride / water; tetrahydrofuran / 3.5 h / 20 °C / cooling with ice

5: hydrogenchloride / 1,4-dioxane; acetonitrile / 4.5 h / 60 °C

6: potassium carbonate / methanol / 1 h / 20 °C

With hydrogenchloride; sodium azide; titanium(III) chloride; sulfuric acid; sulfur trioxide; potassium carbonate; periodic acid; triethylamine; iron(III) chloride; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; acetonitrile;

Reference yield:

: 7205-70-1
(R,S)-1-(ethylsulfinyl)-4-nitrobenzene

: 1223498-81-4
C₁₇H₂₂F₃N₅O₂S

: 1223498-78-9
C₁₇H₂₂F₃N₅O₂S

Guidance literature:: Multi-step reaction with 5 steps

1: sodium azide; sulfur trioxide; sulfuric acid / 6 h / 45 °C / cooling with ice; Inert atmosphere

2: triethylamine / dichloromethane / 3 h / 10 °C / cooling with ice

3: hydrogenchloride; titanium(III) chloride / water; tetrahydrofuran / 3.5 h / 20 °C / cooling with ice

4: hydrogenchloride / 1,4-dioxane; acetonitrile / 4.5 h / 60 °C

5: potassium carbonate / methanol / 1 h / 20 °C

With hydrogenchloride; sodium azide; titanium(III) chloride; sulfuric acid; sulfur trioxide; potassium carbonate; triethylamine; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; acetonitrile;