3-azabicyclo[3.1.0]hexan-6-yl(3,4-dichlorophenyl)methanone O-methyloxime hydrochloride

Base Information

Chemical Name:3-azabicyclo[3.1.0]hexan-6-yl(3,4-dichlorophenyl)methanone O-methyloxime hydrochloride
CAS No.:1370426-46-2
Molecular Formula:C₁₃H₁₄Cl₂N₂O*ClH
Molecular Weight:321.634
Hs Code.:

Synonyms:3-azabicyclo[3.1.0]hexan-6-yl(3,4-dichlorophenyl)methanone O-methyloxime hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-azabicyclo[3.1.0]hexan-6-yl(3,4-dichlorophenyl)methanone O-methyloxime hydrochloride

Chemical Property:

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Technology Process of 3-azabicyclo[3.1.0]hexan-6-yl(3,4-dichlorophenyl)methanone O-methyloxime hydrochloride

There total 5 articles about 3-azabicyclo[3.1.0]hexan-6-yl(3,4-dichlorophenyl)methanone O-methyloxime hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1370426-83-7
tert-butyl 6-((3,4-dichlorophenyl)(methoxyimino)methyl)-3-azabicyclo[3.1.0]hexane-3-carboxylate

: 1370426-46-2
3-azabicyclo[3.1.0]hexan-6-yl(3,4-dichlorophenyl)methanone O-methyloxime hydrochloride

Guidance literature:: With hydrogenchloride; In dichloromethane;

Reference yield:

: 1370426-80-4
tert-butyl 6-(3,4-dichlorobenzoyl)-3-azabicyclo[3.1.0]hexane-3-carboxylate

: 1370426-46-2
3-azabicyclo[3.1.0]hexan-6-yl(3,4-dichlorophenyl)methanone O-methyloxime hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / ethanol / 5 h / Inert atmosphere; Reflux

2: hydrogenchloride / dichloromethane

With pyridine; hydrogenchloride; In ethanol; dichloromethane;

Reference yield:

: 1370426-79-1
tert-butyl 6-((3,4-dichlorophenyl)hydroxymethyl)-3-azabicyclo[3.1.0]hexane-3-carboxylate

: 1370426-46-2
3-azabicyclo[3.1.0]hexan-6-yl(3,4-dichlorophenyl)methanone O-methyloxime hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1 h / -78 °C / Inert atmosphere

2: pyridine / ethanol / 5 h / Inert atmosphere; Reflux

3: hydrogenchloride / dichloromethane

With pyridine; hydrogenchloride; oxalyl dichloride; dimethyl sulfoxide; In ethanol; dichloromethane;