3-azabicyclo[3.1.0]hexan-6-yl(3,4-dichlorophenyl)methanone O-methyl oxime

Base Information

Chemical Name:3-azabicyclo[3.1.0]hexan-6-yl(3,4-dichlorophenyl)methanone O-methyl oxime
CAS No.:1370426-48-4
Molecular Formula:C₁₃H₁₄Cl₂N₂O
Molecular Weight:285.173
Hs Code.:

Synonyms:3-azabicyclo[3.1.0]hexan-6-yl(3,4-dichlorophenyl)methanone O-methyl oxime

Suppliers and Price of 3-azabicyclo[3.1.0]hexan-6-yl(3,4-dichlorophenyl)methanone O-methyl oxime

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-azabicyclo[3.1.0]hexan-6-yl(3,4-dichlorophenyl)methanone O-methyl oxime

Chemical Property:

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Technology Process of 3-azabicyclo[3.1.0]hexan-6-yl(3,4-dichlorophenyl)methanone O-methyl oxime

There total 6 articles about 3-azabicyclo[3.1.0]hexan-6-yl(3,4-dichlorophenyl)methanone O-methyl oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1370426-46-2
3-azabicyclo[3.1.0]hexan-6-yl(3,4-dichlorophenyl)methanone O-methyloxime hydrochloride

: 1370426-48-4
3-azabicyclo[3.1.0]hexan-6-yl(3,4-dichlorophenyl)methanone O-methyl oxime

Guidance literature:: With sodium hydrogencarbonate; In ethyl acetate; at 20 ℃; for 0.5h;

Reference yield:

: 1370426-79-1
tert-butyl 6-((3,4-dichlorophenyl)hydroxymethyl)-3-azabicyclo[3.1.0]hexane-3-carboxylate

: 1370426-48-4
3-azabicyclo[3.1.0]hexan-6-yl(3,4-dichlorophenyl)methanone O-methyl oxime

Guidance literature:: Multi-step reaction with 4 steps

1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1 h / -78 °C / Inert atmosphere

2: pyridine / ethanol / 5 h / Inert atmosphere; Reflux

3: hydrogenchloride / dichloromethane

4: sodium hydrogencarbonate / ethyl acetate / 0.5 h / 20 °C

With pyridine; hydrogenchloride; oxalyl dichloride; sodium hydrogencarbonate; dimethyl sulfoxide; In ethanol; dichloromethane; ethyl acetate;

Reference yield:

: 912468-67-8
tert-butyl 6-formyl-3-azabicyclo[3.1.0]hexane-3-carboxylate

: 1370426-48-4
3-azabicyclo[3.1.0]hexan-6-yl(3,4-dichlorophenyl)methanone O-methyl oxime

Guidance literature:: Multi-step reaction with 5 steps

1: tetrahydrofuran / -78 - 20 °C / Inert atmosphere

2: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1 h / -78 °C / Inert atmosphere

3: pyridine / ethanol / 5 h / Inert atmosphere; Reflux

4: hydrogenchloride / dichloromethane

5: sodium hydrogencarbonate / ethyl acetate / 0.5 h / 20 °C

With pyridine; hydrogenchloride; oxalyl dichloride; sodium hydrogencarbonate; dimethyl sulfoxide; In tetrahydrofuran; ethanol; dichloromethane; ethyl acetate;