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C48H46F2O6

Base Information
  • Chemical Name:C48H46F2O6
  • CAS No.:1413374-43-2
  • Molecular Formula:C48H46F2O6
  • Molecular Weight:756.886
  • Hs Code.:
C<sub>48</sub>H<sub>46</sub>F<sub>2</sub>O<sub>6</sub>

Synonyms:C48H46F2O6

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Chemical Property of C48H46F2O6
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Technology Process of C48H46F2O6

There total 21 articles about C48H46F2O6 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
4-Benzyloxyphenol; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 1h;
C36H35F5O7S; In N,N-dimethyl-formamide; mineral oil; at 0 - 50 ℃;
Guidance literature:
Multi-step reaction with 10 steps
1.1: acetic anhydride; dimethyl sulfoxide / dimethyl sulfoxide / 20 °C / Inert atmosphere
2.1: n-butyllithium / hexane; tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere
2.2: -78 - 0 °C
2.3: cooling with ice
3.1: sodium tetrahydroborate / tetrahydrofuran / 20 °C
4.1: trifluoroacetic anhydride; dimethyl sulfoxide / dichloromethane / 1.5 h / -78 °C
4.2: -78 - 0 °C
5.1: potassium carbonate / 18-crown-6 ether / toluene / 20 °C
6.1: cerium(III) chloride heptahydrate / tetrahydrofuran; methanol / 0.5 h / -23 °C
6.2: 0.75 h
7.1: phosphorus pentoxide / chloroform / 1 h / 20 °C / Inert atmosphere
8.1: sodium methylate; methanol / 20 °C / Industry scale
9.1: pyridine / dichloromethane / 0 - 20 °C / Inert atmosphere
10.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 °C
10.2: 0 - 50 °C
With pyridine; methanol; sodium tetrahydroborate; n-butyllithium; phosphorus pentoxide; cerium(III) chloride heptahydrate; sodium methylate; acetic anhydride; sodium hydride; potassium carbonate; dimethyl sulfoxide; trifluoroacetic anhydride; 18-crown-6 ether; In tetrahydrofuran; methanol; hexane; dichloromethane; chloroform; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene; mineral oil;
Guidance literature:
Multi-step reaction with 10 steps
1.1: cerium(III) chloride heptahydrate / tetrahydrofuran; methanol / 0.5 h / -23 °C
1.2: 0.75 h
2.1: 1H-imidazole / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere
2.2: 12 h / 40 °C
3.1: dimethylsulfide borane complex / tetrahydrofuran / 0 - 20 °C / Inert atmosphere
3.2: 2 h / 0 - 20 °C
4.1: Dess-Martin periodane / dichloromethane / 0 - 20 °C / Inert atmosphere
5.1: hydrogenchloride; methanol / dichloromethane / 20 °C
6.1: pyridine / dmap / dichloromethane / 0.75 h / 0 °C / Inert atmosphere
7.1: diethylamino-sulfur trifluoride / dichloromethane / 16 h / 20 °C / Inert atmosphere
8.1: sodium methylate; methanol / 20 °C / Industry scale
9.1: pyridine / dichloromethane / 0 - 20 °C / Inert atmosphere
10.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 °C
10.2: 0 - 50 °C
With pyridine; 1H-imidazole; hydrogenchloride; methanol; diethylamino-sulfur trifluoride; cerium(III) chloride heptahydrate; dimethylsulfide borane complex; sodium methylate; sodium hydride; Dess-Martin periodane; dmap; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; mineral oil;
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