9b-[(E)-2-(4-Methoxy-phenyl)-vinyl]-1,3-diphenyl-1,9b-dihydro-5-oxa-4-thia-1,2,3a-triaza-cyclopenta[a]naphthalene 4,4-dioxide

Base Information

Chemical Name:9b-[(E)-2-(4-Methoxy-phenyl)-vinyl]-1,3-diphenyl-1,9b-dihydro-5-oxa-4-thia-1,2,3a-triaza-cyclopenta[a]naphthalene 4,4-dioxide
CAS No.:88702-06-1
Molecular Formula:C₂₉H₂₃N₃O₄S
Molecular Weight:509.585
Hs Code.:

Synonyms:9b-[(E)-2-(4-Methoxy-phenyl)-vinyl]-1,3-diphenyl-1,9b-dihydro-5-oxa-4-thia-1,2,3a-triaza-cyclopenta[a]naphthalene 4,4-dioxide

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Chemical Property of 9b-[(E)-2-(4-Methoxy-phenyl)-vinyl]-1,3-diphenyl-1,9b-dihydro-5-oxa-4-thia-1,2,3a-triaza-cyclopenta[a]naphthalene 4,4-dioxide

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Technology Process of 9b-[(E)-2-(4-Methoxy-phenyl)-vinyl]-1,3-diphenyl-1,9b-dihydro-5-oxa-4-thia-1,2,3a-triaza-cyclopenta[a]naphthalene 4,4-dioxide

There total 2 articles about 9b-[(E)-2-(4-Methoxy-phenyl)-vinyl]-1,3-diphenyl-1,9b-dihydro-5-oxa-4-thia-1,2,3a-triaza-cyclopenta[a]naphthalene 4,4-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 88701-89-7
4-[(E)-2-(4-Methoxy-phenyl)-vinyl]-benzo[e][1,2,3]oxathiazine 2,2-dioxide

: 15424-14-3
N-phenylbenzohydrazonoyl chloride

: 88702-06-1
9b-[(E)-2-(4-Methoxy-phenyl)-vinyl]-1,3-diphenyl-1,9b-dihydro-5-oxa-4-thia-1,2,3a-triaza-cyclopenta[a]naphthalene 4,4-dioxide

Guidance literature:: With triethylamine; In benzene; at 50 - 60 ℃; for 36h;

Reference yield:

: 34000-29-8
[E]-3-(p-methoxyphenyl)-1-(2-hydroxyphenyl)prop-2-en-1-one

: 88702-06-1
9b-[(E)-2-(4-Methoxy-phenyl)-vinyl]-1,3-diphenyl-1,9b-dihydro-5-oxa-4-thia-1,2,3a-triaza-cyclopenta[a]naphthalene 4,4-dioxide

Guidance literature:: Multi-step reaction with 2 steps

1: 64 percent / toluene / 4 h / Heating

2: 52 percent / triethylamine / benzene / 36 h / 50 - 60 °C

With triethylamine; In toluene; benzene;