N-(1-(tert-butyldiphenylsilyloxy)-3-hydroxy-2-(hydroxymethyl)propan-2-yl)benzamide

Base Information

Chemical Name:N-(1-(tert-butyldiphenylsilyloxy)-3-hydroxy-2-(hydroxymethyl)propan-2-yl)benzamide
CAS No.:1033408-45-5
Molecular Formula:C₂₇H₃₃NO₄Si
Molecular Weight:463.649
Hs Code.:

Synonyms:N-(1-(tert-butyldiphenylsilyloxy)-3-hydroxy-2-(hydroxymethyl)propan-2-yl)benzamide

Suppliers and Price of N-(1-(tert-butyldiphenylsilyloxy)-3-hydroxy-2-(hydroxymethyl)propan-2-yl)benzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(1-(tert-butyldiphenylsilyloxy)-3-hydroxy-2-(hydroxymethyl)propan-2-yl)benzamide

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Technology Process of N-(1-(tert-butyldiphenylsilyloxy)-3-hydroxy-2-(hydroxymethyl)propan-2-yl)benzamide

There total 1 articles about N-(1-(tert-butyldiphenylsilyloxy)-3-hydroxy-2-(hydroxymethyl)propan-2-yl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1033409-71-0
C₃₀H₃₇NO₄Si

: 1033408-45-5
N-(1-(tert-butyldiphenylsilyloxy)-3-hydroxy-2-(hydroxymethyl)propan-2-yl)benzamide

: 99430-47-4
N-(1,3-dihydroxy-2-(hydroxymethyl)propan-2-yl)benzamide

Guidance literature:: With water; acetic acid; at 60 ℃; for 1h; Inert atmosphere;
DOI:10.1002/chem.200701875

Reference yield: 96.0%

: 1033408-45-5
N-(1-(tert-butyldiphenylsilyloxy)-3-hydroxy-2-(hydroxymethyl)propan-2-yl)benzamide

: 98-88-4
benzoyl chloride

: 1033408-58-0
2-benzamido-3-(tert-butyldiphenylsilyloxy)-2-(hydroxymethyl)propyl benzoate

Guidance literature:: With (4S,4'S,5R,5'R)-2,2'-(propane-2,2-diyl)bis(4,5-diphenyl-4,5-dihydrooxazole); triethylamine; copper dichloride; In tetrahydrofuran; at 20 ℃; for 1h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1002/chem.200701875