2-benzamido-3-(tert-butyldiphenylsilyloxy)-2-(hydroxymethyl)propyl benzoate

Base Information

Chemical Name:2-benzamido-3-(tert-butyldiphenylsilyloxy)-2-(hydroxymethyl)propyl benzoate
CAS No.:1033408-58-0
Molecular Formula:C₃₄H₃₇NO₅Si
Molecular Weight:567.757
Hs Code.:

Synonyms:2-benzamido-3-(tert-butyldiphenylsilyloxy)-2-(hydroxymethyl)propyl benzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-benzamido-3-(tert-butyldiphenylsilyloxy)-2-(hydroxymethyl)propyl benzoate

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Technology Process of 2-benzamido-3-(tert-butyldiphenylsilyloxy)-2-(hydroxymethyl)propyl benzoate

There total 1 articles about 2-benzamido-3-(tert-butyldiphenylsilyloxy)-2-(hydroxymethyl)propyl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1033408-45-5
N-(1-(tert-butyldiphenylsilyloxy)-3-hydroxy-2-(hydroxymethyl)propan-2-yl)benzamide

: 98-88-4
benzoyl chloride

: 1033408-58-0
2-benzamido-3-(tert-butyldiphenylsilyloxy)-2-(hydroxymethyl)propyl benzoate

Guidance literature:: With (4S,4'S,5R,5'R)-2,2'-(propane-2,2-diyl)bis(4,5-diphenyl-4,5-dihydrooxazole); triethylamine; copper dichloride; In tetrahydrofuran; at 20 ℃; for 1h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1002/chem.200701875

Reference yield: 97.0%

: 1033408-58-0
2-benzamido-3-(tert-butyldiphenylsilyloxy)-2-(hydroxymethyl)propyl benzoate

: C₃₄H₃₅NO₄Si

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 0 - 20 ℃; for 1.16667h; Inert atmosphere;
DOI:10.1002/chem.200701875