C₁₅H₁₂F₂N₂O₂

Base Information

Chemical Name:C₁₅H₁₂F₂N₂O₂
CAS No.:1308669-32-0
Molecular Formula:C₁₅H₁₂F₂N₂O₂
Molecular Weight:290.269
Hs Code.:

C<sub>15</sub>H<sub>12</sub>F<sub>2</sub>N<sub>2</sub>O<sub>2</sub>

Synonyms:C₁₅H₁₂F₂N₂O₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₅H₁₂F₂N₂O₂

Chemical Property:

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Technology Process of C₁₅H₁₂F₂N₂O₂

There total 4 articles about C₁₅H₁₂F₂N₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 288067-35-6
4-bromo-2-hydroxy-benzonitrile

: 1308669-33-1
C₁₅H₁₂F₂N₂O₂

: 1308669-32-0
C₁₅H₁₂F₂N₂O₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 0.17 h

1.2: 2.5 h / 20 - 80 °C

2.1: potassium acetate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane / 5 h / 80 °C / Inert atmosphere

3.1: sodium carbonate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / N,N-dimethyl-formamide / 6 h / 100 °C / Inert atmosphere

4.1: ChiralPak OD-H / n-heptane; ethanol / Resolution of racemate

With potassium acetate; sodium carbonate; potassium carbonate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In 1,4-dioxane; ethanol; n-heptane; N,N-dimethyl-formamide; 3.1: Suzuki Coupling;

Reference yield:

: 1308669-31-9
C₁₅H₁₂F₂N₂O₂

: 1308669-33-1
C₁₅H₁₂F₂N₂O₂

: 1308669-32-0
C₁₅H₁₂F₂N₂O₂

Guidance literature:: With ChiralPak OD-H; In ethanol; n-heptane; Resolution of racemate;

Reference yield:

: 1261494-95-4
4-bromo-2-(difluoromethoxy)benzonitrile

: 1308669-33-1
C₁₅H₁₂F₂N₂O₂

: 1308669-32-0
C₁₅H₁₂F₂N₂O₂

Guidance literature:: Multi-step reaction with 3 steps

1: potassium acetate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane / 5 h / 80 °C / Inert atmosphere

2: sodium carbonate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / N,N-dimethyl-formamide / 6 h / 100 °C / Inert atmosphere

3: ChiralPak OD-H / n-heptane; ethanol / Resolution of racemate

With potassium acetate; sodium carbonate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In 1,4-dioxane; ethanol; n-heptane; N,N-dimethyl-formamide; 2: Suzuki Coupling;