(1S,5S)-5-methyl-2-(2-phenylprop-2-yl)cyclohexyl (E)-3,7-dimethylocta-2,6-dienoate

Base Information

Chemical Name:(1S,5S)-5-methyl-2-(2-phenylprop-2-yl)cyclohexyl (E)-3,7-dimethylocta-2,6-dienoate
CAS No.:1335013-09-6
Molecular Formula:C₂₆H₃₈O₂
Molecular Weight:382.587
Hs Code.:

Synonyms:(1S,5S)-5-methyl-2-(2-phenylprop-2-yl)cyclohexyl (E)-3,7-dimethylocta-2,6-dienoate

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Chemical Property of (1S,5S)-5-methyl-2-(2-phenylprop-2-yl)cyclohexyl (E)-3,7-dimethylocta-2,6-dienoate

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Technology Process of (1S,5S)-5-methyl-2-(2-phenylprop-2-yl)cyclohexyl (E)-3,7-dimethylocta-2,6-dienoate

There total 2 articles about (1S,5S)-5-methyl-2-(2-phenylprop-2-yl)cyclohexyl (E)-3,7-dimethylocta-2,6-dienoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 110-93-0,129085-68-3
6-Methyl-hept-5-en-2-on

: 1335013-07-4
(1S,2R,5S)-5-methyl-2-(2-phenylpropan-2-yl)cyclohexyl-2-(diethoxyphosphoryl)-acetate

: C₂₆H₃₈O₂

: 1335013-09-6
(1S,5S)-5-methyl-2-(2-phenylprop-2-yl)cyclohexyl (E)-3,7-dimethylocta-2,6-dienoate

Guidance literature:: (1S,2R,5S)-5-methyl-2-(2-phenylpropan-2-yl)cyclohexyl-2-(diethoxyphosphoryl)-acetate; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 0.116667h; Inert atmosphere;

6-Methyl-hept-5-en-2-on; In tetrahydrofuran; at 20 ℃; for 4h; Inert atmosphere;
DOI:10.1002/ejoc.201100400

Reference yield:

: 57707-91-2
(1S,2R,5S)-8-(+)-phenylmenthol

: 1335013-09-6
(1S,5S)-5-methyl-2-(2-phenylprop-2-yl)cyclohexyl (E)-3,7-dimethylocta-2,6-dienoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: dmap / toluene / 140 h / Reflux; Inert atmosphere

2.1: sodium hydride / tetrahydrofuran / 0.12 h / 0 °C / Inert atmosphere

2.2: 4 h / 20 °C / Inert atmosphere

With dmap; sodium hydride; In tetrahydrofuran; toluene; 2.1: Wadsworth-Emmons condensation;
DOI:10.1002/ejoc.201100400