(1S,2R,5S)-5-methyl-2-(2-phenylpropan-2-yl)cyclohexyl-2-(diethoxyphosphoryl)-acetate

Base Information

Chemical Name:(1S,2R,5S)-5-methyl-2-(2-phenylpropan-2-yl)cyclohexyl-2-(diethoxyphosphoryl)-acetate
CAS No.:1335013-07-4
Molecular Formula:C₂₂H₃₅O₅P
Molecular Weight:410.491
Hs Code.:

Synonyms:(1S,2R,5S)-5-methyl-2-(2-phenylpropan-2-yl)cyclohexyl-2-(diethoxyphosphoryl)-acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,2R,5S)-5-methyl-2-(2-phenylpropan-2-yl)cyclohexyl-2-(diethoxyphosphoryl)-acetate

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Technology Process of (1S,2R,5S)-5-methyl-2-(2-phenylpropan-2-yl)cyclohexyl-2-(diethoxyphosphoryl)-acetate

There total 1 articles about (1S,2R,5S)-5-methyl-2-(2-phenylpropan-2-yl)cyclohexyl-2-(diethoxyphosphoryl)-acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 867-13-0
diethoxyphosphoryl-acetic acid ethyl ester

: 57707-91-2
(1S,2R,5S)-8-(+)-phenylmenthol

: 1335013-07-4
(1S,2R,5S)-5-methyl-2-(2-phenylpropan-2-yl)cyclohexyl-2-(diethoxyphosphoryl)-acetate

Guidance literature:: With dmap; In toluene; for 140h; Reflux; Inert atmosphere;
DOI:10.1002/ejoc.201100400

Reference yield: 30.0%

: 34837-55-3
Phenylselenyl bromide

: 1335013-07-4
(1S,2R,5S)-5-methyl-2-(2-phenylpropan-2-yl)cyclohexyl-2-(diethoxyphosphoryl)-acetate

: 74-88-4
methyl iodide

: 2-(diethoxy-phosphoryl)-2-phenylselanyl-propionic acid (1S,2R,5S)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester

Guidance literature:: (1S,2R,5S)-5-methyl-2-(2-phenylpropan-2-yl)cyclohexyl-2-(diethoxyphosphoryl)-acetate; With potassium tert-butylate; In dimethyl sulfoxide; at 0 - 20 ℃; Inert atmosphere;

Phenylselenyl bromide; In dimethyl sulfoxide; at 60 ℃; for 4h; Inert atmosphere;

methyl iodide;
DOI:10.1016/j.tetasy.2012.11.021

Reference yield:

: 110-93-0,129085-68-3
6-Methyl-hept-5-en-2-on

: 1335013-07-4
(1S,2R,5S)-5-methyl-2-(2-phenylpropan-2-yl)cyclohexyl-2-(diethoxyphosphoryl)-acetate

: C₂₆H₃₈O₂

: 1335013-09-6
(1S,5S)-5-methyl-2-(2-phenylprop-2-yl)cyclohexyl (E)-3,7-dimethylocta-2,6-dienoate

Guidance literature:: (1S,2R,5S)-5-methyl-2-(2-phenylpropan-2-yl)cyclohexyl-2-(diethoxyphosphoryl)-acetate; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 0.116667h; Inert atmosphere;

6-Methyl-hept-5-en-2-on; In tetrahydrofuran; at 20 ℃; for 4h; Inert atmosphere;
DOI:10.1002/ejoc.201100400