5-<2-(methoxycarbonyl)-1-(p-methoxyphenyl)ethyl>-2,3,4,6-tetramethoxyacetophenone

Base Information

Chemical Name:5-<2-(methoxycarbonyl)-1-(p-methoxyphenyl)ethyl>-2,3,4,6-tetramethoxyacetophenone
CAS No.:133466-29-2
Molecular Formula:C₂₃H₂₈O₈
Molecular Weight:432.471
Hs Code.:

Synonyms:5-<2-(methoxycarbonyl)-1-(p-methoxyphenyl)ethyl>-2,3,4,6-tetramethoxyacetophenone

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Chemical Property of 5-<2-(methoxycarbonyl)-1-(p-methoxyphenyl)ethyl>-2,3,4,6-tetramethoxyacetophenone

Chemical Property:

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Technology Process of 5-<2-(methoxycarbonyl)-1-(p-methoxyphenyl)ethyl>-2,3,4,6-tetramethoxyacetophenone

There total 1 articles about 5-<2-(methoxycarbonyl)-1-(p-methoxyphenyl)ethyl>-2,3,4,6-tetramethoxyacetophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 133466-28-1
6-acetyl-3,4-dihydro-5,7,8-trihydroxy-4-(p-methoxyphenyl)coumarin

: 77-78-1
dimethyl sulfate

: 133466-29-2
5-<2-(methoxycarbonyl)-1-(p-methoxyphenyl)ethyl>-2,3,4,6-tetramethoxyacetophenone

Guidance literature:: With potassium carbonate; In water; acetone; for 30h; Heating;
DOI:10.1246/bcsj.64.309

Reference yield: 90.0%

: 133466-29-2
5-<2-(methoxycarbonyl)-1-(p-methoxyphenyl)ethyl>-2,3,4,6-tetramethoxyacetophenone

: 123-11-5
4-methoxy-benzaldehyde

: 5'-<2-carboxy-1-(p-methoxyphenyl)ethyl>-2',3',4,4',6'-pentamethoxychalcone

Guidance literature:: With sodium hydroxide; In methanol; for 96h; Ambient temperature;
DOI:10.1246/bcsj.64.309

Reference yield:

: 133466-29-2
5-<2-(methoxycarbonyl)-1-(p-methoxyphenyl)ethyl>-2,3,4,6-tetramethoxyacetophenone

: 133574-63-7
5'-<2-(methoxycarbonyl)-1-(p-methoxyphenyl)ethyl>-2',3',4,4',6'-pentamethoxychalcone

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / 50percent aq. NaOH / methanol / 96 h / Ambient temperature

2: 100 percent / diethyl ether / Ambient temperature

With sodium hydroxide; In methanol; diethyl ether;
DOI:10.1246/bcsj.64.309