benzyl (2S,3S,3aS,4aS,5R,8S,8aR)-5,10,10-trimethyl-5,8-methano-2,3-propano-octahydroisoxazolo[3,2-b]benzoxazole-3-carboxylate

Base Information

Chemical Name:benzyl (2S,3S,3aS,4aS,5R,8S,8aR)-5,10,10-trimethyl-5,8-methano-2,3-propano-octahydroisoxazolo[3,2-b]benzoxazole-3-carboxylate
CAS No.:503549-97-1
Molecular Formula:C₂₄H₃₁NO₄
Molecular Weight:397.514
Hs Code.:

Synonyms:benzyl (2S,3S,3aS,4aS,5R,8S,8aR)-5,10,10-trimethyl-5,8-methano-2,3-propano-octahydroisoxazolo[3,2-b]benzoxazole-3-carboxylate

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Chemical Property of benzyl (2S,3S,3aS,4aS,5R,8S,8aR)-5,10,10-trimethyl-5,8-methano-2,3-propano-octahydroisoxazolo[3,2-b]benzoxazole-3-carboxylate

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Technology Process of benzyl (2S,3S,3aS,4aS,5R,8S,8aR)-5,10,10-trimethyl-5,8-methano-2,3-propano-octahydroisoxazolo[3,2-b]benzoxazole-3-carboxylate

There total 3 articles about benzyl (2S,3S,3aS,4aS,5R,8S,8aR)-5,10,10-trimethyl-5,8-methano-2,3-propano-octahydroisoxazolo[3,2-b]benzoxazole-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 87995-31-1
benzyl 1-cyclopentene-1-carboxylate

: 154460-64-7
(+)-3-hydroxyaminoisoborneol*HCl

: 149-73-5
trimethyl orthoformate

: 503549-97-1
benzyl (2S,3S,3aS,4aS,5R,8S,8aR)-5,10,10-trimethyl-5,8-methano-2,3-propano-octahydroisoxazolo[3,2-b]benzoxazole-3-carboxylate

Guidance literature:: (+)-3-hydroxyaminoisoborneol*HCl; trimethyl orthoformate; With calcium carbonate; In toluene; at 45 ℃; for 4h;

benzyl 1-cyclopentene-1-carboxylate; In dichloromethane; at 60 ℃; for 16h;
DOI:10.1002/1099-0690(200211)2002:21<3566::AID-EJOC3566>3.0.CO;2-F

Reference yield:

: 1560-11-8
cyclopent-1-enecarboxylic acid

: 503549-97-1
benzyl (2S,3S,3aS,4aS,5R,8S,8aR)-5,10,10-trimethyl-5,8-methano-2,3-propano-octahydroisoxazolo[3,2-b]benzoxazole-3-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 98 percent / 4-(dimethylamino)pyridine; dicyclohexylcarbodiimide / CH₂Cl₂ / 24 h / 20 °C

2.1: calcium carbonate / toluene / 4 h / 45 °C

2.2: 50 percent / CH₂Cl₂ / 16 h / 60 °C

With dmap; dicyclohexyl-carbodiimide; calcium carbonate; In dichloromethane; toluene;
DOI:10.1002/1099-0690(200211)2002:21<3566::AID-EJOC3566>3.0.CO;2-F

Reference yield:

: 100-51-6,185532-71-2
benzyl alcohol

: 503549-97-1
benzyl (2S,3S,3aS,4aS,5R,8S,8aR)-5,10,10-trimethyl-5,8-methano-2,3-propano-octahydroisoxazolo[3,2-b]benzoxazole-3-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 98 percent / 4-(dimethylamino)pyridine; dicyclohexylcarbodiimide / CH₂Cl₂ / 24 h / 20 °C

2.1: calcium carbonate / toluene / 4 h / 45 °C

2.2: 50 percent / CH₂Cl₂ / 16 h / 60 °C

With dmap; dicyclohexyl-carbodiimide; calcium carbonate; In dichloromethane; toluene;
DOI:10.1002/1099-0690(200211)2002:21<3566::AID-EJOC3566>3.0.CO;2-F