2-(4-benzyloxy-2-nitro-benzenesulfonylamino)-hexanedioic acid 1-tert-butyl ester 6-methyl ester

Base Information

Chemical Name:2-(4-benzyloxy-2-nitro-benzenesulfonylamino)-hexanedioic acid 1-tert-butyl ester 6-methyl ester
CAS No.:1026968-07-9
Molecular Formula:C₂₄H₃₀N₂O₉S
Molecular Weight:522.576
Hs Code.:

2-(4-benzyloxy-2-nitro-benzenesulfonylamino)-hexanedioic acid 1-<i>tert</i>-butyl ester 6-methyl ester

Synonyms:2-(4-benzyloxy-2-nitro-benzenesulfonylamino)-hexanedioic acid 1-tert-butyl ester 6-methyl ester

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Chemical Property of 2-(4-benzyloxy-2-nitro-benzenesulfonylamino)-hexanedioic acid 1-tert-butyl ester 6-methyl ester

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Technology Process of 2-(4-benzyloxy-2-nitro-benzenesulfonylamino)-hexanedioic acid 1-tert-butyl ester 6-methyl ester

There total 4 articles about 2-(4-benzyloxy-2-nitro-benzenesulfonylamino)-hexanedioic acid 1-tert-butyl ester 6-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2-amino-hexanedioic acid 1-tert-butyl ester 6-methyl ester

: 238405-67-9
4-benzyloxy-2-nitrobenzenesulfonyl chloride

: 1026968-07-9
2-(4-benzyloxy-2-nitro-benzenesulfonylamino)-hexanedioic acid 1-tert-butyl ester 6-methyl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 ℃;
DOI:10.1021/jm020475w

Reference yield:

: 610-81-1
4-hydroxy-2-nitroaniline

: 1026968-07-9
2-(4-benzyloxy-2-nitro-benzenesulfonylamino)-hexanedioic acid 1-tert-butyl ester 6-methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium tert-butoxide / dimethylformamide / 0.5 h / 0 °C

1.2: 81 percent / dimethylformamide / 0.5 h / 0 °C

2.1: TFA; aq. HCl; NaNO₂ / 0.08 h / 0 °C

2.2: 75 percent / aq. AcOH; H₂SO₃; CuCl₂ / CuCl / 0.58 h / 20 °C

3.1: diisopropylethylamine / CH₂Cl₂ / 0 °C

With hydrogenchloride; potassium tert-butylate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; sodium nitrite; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm020475w

Reference yield:

: 26697-35-8
4-benzyloxy-2-nitroaniline

: 1026968-07-9
2-(4-benzyloxy-2-nitro-benzenesulfonylamino)-hexanedioic acid 1-tert-butyl ester 6-methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: TFA; aq. HCl; NaNO₂ / 0.08 h / 0 °C

1.2: 75 percent / aq. AcOH; H₂SO₃; CuCl₂ / CuCl / 0.58 h / 20 °C

2.1: diisopropylethylamine / CH₂Cl₂ / 0 °C

With hydrogenchloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; sodium nitrite; In dichloromethane;
DOI:10.1021/jm020475w