(+/-)-N-[2-[[[[2,6-bis(1-methylethyl)phenyl]amino]carbonyl]amino]-1-phenylethyl]-4-methoxybenzenecarboxamide

Base Information

Chemical Name:(+/-)-N-[2-[[[[2,6-bis(1-methylethyl)phenyl]amino]carbonyl]amino]-1-phenylethyl]-4-methoxybenzenecarboxamide
CAS No.:137102-02-4
Molecular Formula:C₂₉H₃₅N₃O₃
Molecular Weight:473.615
Hs Code.:

Synonyms:(+/-)-N-[2-[[[[2,6-bis(1-methylethyl)phenyl]amino]carbonyl]amino]-1-phenylethyl]-4-methoxybenzenecarboxamide

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Chemical Property of (+/-)-N-[2-[[[[2,6-bis(1-methylethyl)phenyl]amino]carbonyl]amino]-1-phenylethyl]-4-methoxybenzenecarboxamide

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Technology Process of (+/-)-N-[2-[[[[2,6-bis(1-methylethyl)phenyl]amino]carbonyl]amino]-1-phenylethyl]-4-methoxybenzenecarboxamide

There total 4 articles about (+/-)-N-[2-[[[[2,6-bis(1-methylethyl)phenyl]amino]carbonyl]amino]-1-phenylethyl]-4-methoxybenzenecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 14062-83-0
N-[cyano(phenyl)methyl]-4-methoxybenzamide

: 137102-02-4
(+/-)-N-[2-[[[[2,6-bis(1-methylethyl)phenyl]amino]carbonyl]amino]-1-phenylethyl]-4-methoxybenzenecarboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: NH₃, H₂ / Ranney nickel / methanol / 2585.7 Torr / Ambient temperature

2: tetrahydrofuran / 2 h / Ambient temperature

With ammonia; hydrogen; ranney nickel; In tetrahydrofuran; methanol;
DOI:10.1021/jm00038a010

Reference yield:

: 100-07-2
4-methoxy-benzoyl chloride

: 137102-02-4
(+/-)-N-[2-[[[[2,6-bis(1-methylethyl)phenyl]amino]carbonyl]amino]-1-phenylethyl]-4-methoxybenzenecarboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N / tetrahydrofuran / 2 h / Ambient temperature

2: NH₃, H₂ / Ranney nickel / methanol / 2585.7 Torr / Ambient temperature

3: tetrahydrofuran / 2 h / Ambient temperature

With ammonia; hydrogen; triethylamine; ranney nickel; In tetrahydrofuran; methanol;
DOI:10.1021/jm00038a010

Reference yield:

: 16750-42-8,41804-94-8
2-amino-2-phenylacetonitrile

: 137102-02-4
(+/-)-N-[2-[[[[2,6-bis(1-methylethyl)phenyl]amino]carbonyl]amino]-1-phenylethyl]-4-methoxybenzenecarboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N / tetrahydrofuran / 2 h / Ambient temperature

2: NH₃, H₂ / Ranney nickel / methanol / 2585.7 Torr / Ambient temperature

3: tetrahydrofuran / 2 h / Ambient temperature

With ammonia; hydrogen; triethylamine; ranney nickel; In tetrahydrofuran; methanol;
DOI:10.1021/jm00038a010