(4S,5S)-5-[2-(2-Dodecyl-[1,3]dioxolan-2-yl)-ethyl]-4-methyl-oxazolidine-3-carboxylic acid cyclohexyl ester

Base Information

Chemical Name:(4S,5S)-5-[2-(2-Dodecyl-[1,3]dioxolan-2-yl)-ethyl]-4-methyl-oxazolidine-3-carboxylic acid cyclohexyl ester
CAS No.:126260-88-6
Molecular Formula:C₂₈H₅₁NO₅
Molecular Weight:481.717
Hs Code.:

Synonyms:(4S,5S)-5-[2-(2-Dodecyl-[1,3]dioxolan-2-yl)-ethyl]-4-methyl-oxazolidine-3-carboxylic acid cyclohexyl ester

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Chemical Property of (4S,5S)-5-[2-(2-Dodecyl-[1,3]dioxolan-2-yl)-ethyl]-4-methyl-oxazolidine-3-carboxylic acid cyclohexyl ester

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Technology Process of (4S,5S)-5-[2-(2-Dodecyl-[1,3]dioxolan-2-yl)-ethyl]-4-methyl-oxazolidine-3-carboxylic acid cyclohexyl ester

There total 9 articles about (4S,5S)-5-[2-(2-Dodecyl-[1,3]dioxolan-2-yl)-ethyl]-4-methyl-oxazolidine-3-carboxylic acid cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 107-21-1
ethylene glycol

: 126260-85-3
(4R,5R)-4-Methyl-5-(3-oxo-pentadecyl)-oxazolidine-3-carboxylic acid cyclohexyl ester

: 126260-88-6
(4S,5S)-5-[2-(2-Dodecyl-[1,3]dioxolan-2-yl)-ethyl]-4-methyl-oxazolidine-3-carboxylic acid cyclohexyl ester

Guidance literature:: With toluene-4-sulfonic acid; In benzene; Heating;

Reference yield:

: 1124-54-5
carbamic acid cyclohexyl ester

: 126260-88-6
(4S,5S)-5-[2-(2-Dodecyl-[1,3]dioxolan-2-yl)-ethyl]-4-methyl-oxazolidine-3-carboxylic acid cyclohexyl ester

Guidance literature:: Multi-step reaction with 8 steps

1: sodium carbonate

2: 53 percent / p-TsOH / diethyl ether / 0.67 h / Heating

3: 1.) Hg(OAc)2, 2.) NaBH₄, KOH / 1.) CH₃CN, 2.) CH₂Cl₂

4: 100 percent / H₂ / 10percent Pd/C / ethanol

5: 87 percent / PCC / CH₂Cl₂

6: 63 percent

7: 98 percent / Jones' reagent

8: 96 percent / p-TsOH / benzene / Heating

With potassium hydroxide; sodium tetrahydroborate; jones' reagent; mercury(II) diacetate; hydrogen; sodium carbonate; toluene-4-sulfonic acid; pyridinium chlorochromate; palladium on activated charcoal; In diethyl ether; ethanol; dichloromethane; benzene;

Reference yield:

: 60794-21-0
cyclohexyl (N-hydroxymethyl)carbamate

: 126260-88-6
(4S,5S)-5-[2-(2-Dodecyl-[1,3]dioxolan-2-yl)-ethyl]-4-methyl-oxazolidine-3-carboxylic acid cyclohexyl ester

Guidance literature:: Multi-step reaction with 7 steps

1: 53 percent / p-TsOH / diethyl ether / 0.67 h / Heating

2: 1.) Hg(OAc)2, 2.) NaBH₄, KOH / 1.) CH₃CN, 2.) CH₂Cl₂

3: 100 percent / H₂ / 10percent Pd/C / ethanol

4: 87 percent / PCC / CH₂Cl₂

5: 63 percent

6: 98 percent / Jones' reagent

7: 96 percent / p-TsOH / benzene / Heating

With potassium hydroxide; sodium tetrahydroborate; jones' reagent; mercury(II) diacetate; hydrogen; toluene-4-sulfonic acid; pyridinium chlorochromate; palladium on activated charcoal; In diethyl ether; ethanol; dichloromethane; benzene;