diiron(I) dinitrogen (2,2,6,6-tetramethyl-3,5-bis(diisopropylphenylimido)-hept-4-yl-1H)2

Base Information

• Chemical Name: diiron(I) dinitrogen (2,2,6,6-tetramethyl-3,5-bis(diisopropylphenylimido)-hept-4-yl-1H)2
• CAS No.: 368862-39-9
• Molecular Formula: C₇₀H₁₀₆Fe₂N₆
• Molecular Weight: 1143.35

Synonyms:diiron(I) dinitrogen (2,2,6,6-tetramethyl-3,5-bis(diisopropylphenylimido)-hept-4-yl-1H)2

Chemical Property of diiron(I) dinitrogen (2,2,6,6-tetramethyl-3,5-bis(diisopropylphenylimido)-hept-4-yl-1H)2

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Technology Process of diiron(I) dinitrogen (2,2,6,6-tetramethyl-3,5-bis(diisopropylphenylimido)-hept-4-yl-1H)2

There total 2 articles about diiron(I) dinitrogen (2,2,6,6-tetramethyl-3,5-bis(diisopropylphenylimido)-hept-4-yl-1H)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

(2,2,6,6-tetramethyl-3,5-bis(2,6-diisopropylphenylimido)hept-4-yl)iron(II) chloride (415701-46-1) → diiron(I) dinitrogen (2,2,6,6-tetramethyl-3,5-bis(diisopropylphenylimido)-hept-4-yl-1H)2 (368862-39-9)

Guidance literature:

With naphthalenide; In not given; complex was reducted with naphthalenide under N2;

DOI:10.1021/ja016094+

Reference yield:

((((CH3)2CH)2C6H3)2((CH3)3C)2C3HN2)FeClK((CH2CH2)6O6) + nitrogen (7727-37-9) → diiron(I) dinitrogen (2,2,6,6-tetramethyl-3,5-bis(diisopropylphenylimido)-hept-4-yl-1H)2 (368862-39-9)

Guidance literature:

In not given; 3 d; not isolated;

DOI:10.1016/j.jorganchem.2009.04.005

Reference yield: 74.0%

diiron(I) dinitrogen (2,2,6,6-tetramethyl-3,5-bis(diisopropylphenylimido)-hept-4-yl-1H)2 (368862-39-9) + 2,4,6-trimethylaniline azide (14213-00-4) → C44H64FeN3

Guidance literature:

In tetrahydrofuran; at 23 ℃; for 0.25h;

DOI:10.1021/acs.organomet.1c00454

upstream raw materials:

(2,2,6,6-tetramethyl-3,5-bis(2,6-diisopropylphenylimido)hept-4-yl)iron(II) chloride

nitrogen

Downstream raw materials:

[Fe(2,6-diisopropylphenylNC(tert-butyl)CHC(tert-butyl)N-2,6-diisopropylphenyl)]2O

Fe(CH(C₆H₃(CH(CH₃)2)2NC(C(CH₃)3))2)NC₆H₅NC₆H₅

iron(III)(2,2,6,6-tetramethyl-3,5-bis(diisopropylphenylimido)-hept-4-yl-1H)(N-1-adamantyl)

[(i-Pr2C6H3NC(Me)CHC(Me)NC6H3-i-Pr2)Fe]2(μ-N3-1-adamantyl)

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