tert-butyldimethylsilyl 2-{[3-(tert-butyldimethylsilyl)oxy]propyl}-3,5,6-trimethyl-4-(phenylsulfinyl)phenyl ether

Base Information

Chemical Name:tert-butyldimethylsilyl 2-{[3-(tert-butyldimethylsilyl)oxy]propyl}-3,5,6-trimethyl-4-(phenylsulfinyl)phenyl ether
CAS No.:173069-18-6
Molecular Formula:C₃₀H₅₀O₃SSi₂
Molecular Weight:546.962
Hs Code.:

Synonyms:tert-butyldimethylsilyl 2-{[3-(tert-butyldimethylsilyl)oxy]propyl}-3,5,6-trimethyl-4-(phenylsulfinyl)phenyl ether

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Chemical Property of tert-butyldimethylsilyl 2-{[3-(tert-butyldimethylsilyl)oxy]propyl}-3,5,6-trimethyl-4-(phenylsulfinyl)phenyl ether

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Technology Process of tert-butyldimethylsilyl 2-{[3-(tert-butyldimethylsilyl)oxy]propyl}-3,5,6-trimethyl-4-(phenylsulfinyl)phenyl ether

There total 5 articles about tert-butyldimethylsilyl 2-{[3-(tert-butyldimethylsilyl)oxy]propyl}-3,5,6-trimethyl-4-(phenylsulfinyl)phenyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1026089-34-8
1-(tert-Butyl-dimethyl-silanyloxy)-2-[3-(tert-butyl-dimethyl-silanyloxy)-propyl]-3,5,6-trimethyl-4-phenylsulfanyl-benzene

: 173069-18-6
tert-butyldimethylsilyl 2-{[3-(tert-butyldimethylsilyl)oxy]propyl}-3,5,6-trimethyl-4-(phenylsulfinyl)phenyl ether

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at -50 - -30 ℃; for 1.5h; Yield given;
DOI:10.1021/jo970418o

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 173069-18-6
tert-butyldimethylsilyl 2-{[3-(tert-butyldimethylsilyl)oxy]propyl}-3,5,6-trimethyl-4-(phenylsulfinyl)phenyl ether

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / imidazole / dimethylformamide / 30 h / Ambient temperature

2: tetrahydrofuran; diethyl ether / 1 h / -50 °C

3: m-CPBA / CH₂Cl₂ / 1.5 h / -50 - -30 °C

With 1H-imidazole; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo970418o

Reference yield:

: 100-58-3
phenylmagnesium bromide

: 173069-18-6
tert-butyldimethylsilyl 2-{[3-(tert-butyldimethylsilyl)oxy]propyl}-3,5,6-trimethyl-4-(phenylsulfinyl)phenyl ether

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran; diethyl ether / 1 h / -50 °C

2: m-CPBA / CH₂Cl₂ / 1.5 h / -50 - -30 °C

With 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/jo970418o