(R,R)-N-tert-butoxycarbonyl-N'-(4-nitrophenylsulfonyl)-1,2-diphenylethylenediamine

Base Information

Chemical Name:(R,R)-N-tert-butoxycarbonyl-N'-(4-nitrophenylsulfonyl)-1,2-diphenylethylenediamine
CAS No.:450368-81-7
Molecular Formula:C₂₅H₂₇N₃O₆S
Molecular Weight:497.572
Hs Code.:

Synonyms:(R,R)-N-tert-butoxycarbonyl-N'-(4-nitrophenylsulfonyl)-1,2-diphenylethylenediamine

Suppliers and Price of (R,R)-N-tert-butoxycarbonyl-N'-(4-nitrophenylsulfonyl)-1,2-diphenylethylenediamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R,R)-N-tert-butoxycarbonyl-N'-(4-nitrophenylsulfonyl)-1,2-diphenylethylenediamine

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Technology Process of (R,R)-N-tert-butoxycarbonyl-N'-(4-nitrophenylsulfonyl)-1,2-diphenylethylenediamine

There total 2 articles about (R,R)-N-tert-butoxycarbonyl-N'-(4-nitrophenylsulfonyl)-1,2-diphenylethylenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 450368-80-6
N-((1R,2R)-2-amino-1,2-diphenylethyl)-4-nitrobenzenesulfonamide

: 450368-81-7
(R,R)-N-tert-butoxycarbonyl-N'-(4-nitrophenylsulfonyl)-1,2-diphenylethylenediamine

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 24h;
DOI:10.1021/jo0257795

Reference yield:

: 98-74-8
4-Nitrobenzenesulfonyl chloride

: 450368-81-7
(R,R)-N-tert-butoxycarbonyl-N'-(4-nitrophenylsulfonyl)-1,2-diphenylethylenediamine

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / NEt₃ / CH₂Cl₂ / 20 °C

2: 99 percent / DIPEA / CH₂Cl₂ / 24 h / 20 °C

With triethylamine; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1021/jo0257795