Dimethylthiocarbamoylsulfanylmethyl-triphenyl-phosphonium; chloride

Base Information

• Chemical Name: Dimethylthiocarbamoylsulfanylmethyl-triphenyl-phosphonium; chloride
• CAS No.: 110637-64-4
• Molecular Formula: C₂₂H₂₃NPS₂*Cl
• Molecular Weight: 431.99
• Mol file: 110637-64-4.mol

Synonyms:Dimethylthiocarbamoylsulfanylmethyl-triphenyl-phosphonium; chloride

Chemical Property of Dimethylthiocarbamoylsulfanylmethyl-triphenyl-phosphonium; chloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Dimethylthiocarbamoylsulfanylmethyl-triphenyl-phosphonium; chloride

There total 2 articles about Dimethylthiocarbamoylsulfanylmethyl-triphenyl-phosphonium; chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.2%

chloromethyltriphenylphosphonium chloride (5293-84-5) + sodium dimethyldithiocarbamate (128-04-1) → Dimethylthiocarbamoylsulfanylmethyl-triphenyl-phosphonium; chloride (110637-64-4)

Guidance literature:

In chloroform; for 8h; Ambient temperature;

DOI:10.1021/jo00233a008

Reference yield: 80.0%

chloromethyltriphenylphosphonium chloride (5293-84-5) + Benzyltriphenylphosphonium dimethyldithiocarbamate (110637-73-5) → benzyltriphenylphosphonium chloride (1100-88-5) + Dimethylthiocarbamoylsulfanylmethyl-triphenyl-phosphonium; chloride (110637-64-4)

Guidance literature:

In 1,2-dimethoxyethane; for 2.5h; Ambient temperature;

DOI:10.1021/jo00233a008

Reference yield: 100.0%

Dimethylthiocarbamoylsulfanylmethyl-triphenyl-phosphonium; chloride (110637-64-4) → Dimethylthiocarbamoylsulfanylmethyl-triphenyl-phosphonium; iodide (110637-62-2)

Guidance literature:

With sodium iodide; In chloroform; for 3h; Ambient temperature;

DOI:10.1021/jo00233a008

upstream raw materials:

chloromethyltriphenylphosphonium chloride

sodium dimethyldithiocarbamate

Benzyltriphenylphosphonium dimethyldithiocarbamate

Downstream raw materials:

Dimethylthiocarbamoylsulfanylmethyl-triphenyl-phosphonium; iodide

triphenylphosphorane