cis-(+)-2-(4'-methoxyphenyl)-3-acetyloxy-2,3-dihydro-1,5-benzothiazepine-4(5H)-one

Base Information

Chemical Name:cis-(+)-2-(4'-methoxyphenyl)-3-acetyloxy-2,3-dihydro-1,5-benzothiazepine-4(5H)-one
CAS No.:132748-48-2
Molecular Formula:C₁₈H₁₇NO₄S
Molecular Weight:343.403
Hs Code.:

Synonyms:cis-(+)-2-(4'-methoxyphenyl)-3-acetyloxy-2,3-dihydro-1,5-benzothiazepine-4(5H)-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cis-(+)-2-(4'-methoxyphenyl)-3-acetyloxy-2,3-dihydro-1,5-benzothiazepine-4(5H)-one

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Technology Process of cis-(+)-2-(4'-methoxyphenyl)-3-acetyloxy-2,3-dihydro-1,5-benzothiazepine-4(5H)-one

There total 2 articles about cis-(+)-2-(4'-methoxyphenyl)-3-acetyloxy-2,3-dihydro-1,5-benzothiazepine-4(5H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 132748-48-2
cis-(+)-2-(4'-methoxyphenyl)-3-acetyloxy-2,3-dihydro-1,5-benzothiazepine-4(5H)-one

Guidance literature:

Reference yield: 71.0%

: 42399-51-9
cis-(+)-2-(4'-methoxyphenyl)-3-hydroxy-2,3-dihydro-1,5-benzothiazepine-4(5H)-one

: 75-36-5
acetyl chloride

: 132748-48-2
cis-(+)-2-(4'-methoxyphenyl)-3-acetyloxy-2,3-dihydro-1,5-benzothiazepine-4(5H)-one

Guidance literature:: With pyridine; In ice-water;

Reference yield:

: 4584-46-7
(2-chloroethyl)dimethylamine hydrochloride

: 132748-48-2
cis-(+)-2-(4'-methoxyphenyl)-3-acetyloxy-2,3-dihydro-1,5-benzothiazepine-4(5H)-one

: 42399-41-7
diltiazem

Guidance literature:: With hydrogenchloride; calcium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; In dichloromethane; water; isopropyl alcohol;