(2S,3S)-2-tert-Butoxycarbonylamino-3-(tert-butyl-dimethyl-silanyloxy)-succinic acid 4-benzyl ester

Base Information

Chemical Name:(2S,3S)-2-tert-Butoxycarbonylamino-3-(tert-butyl-dimethyl-silanyloxy)-succinic acid 4-benzyl ester
CAS No.:207510-42-7
Molecular Formula:C₂₂H₃₅NO₇Si
Molecular Weight:453.608
Hs Code.:

Synonyms:(2S,3S)-2-tert-Butoxycarbonylamino-3-(tert-butyl-dimethyl-silanyloxy)-succinic acid 4-benzyl ester

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Chemical Property of (2S,3S)-2-tert-Butoxycarbonylamino-3-(tert-butyl-dimethyl-silanyloxy)-succinic acid 4-benzyl ester

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Technology Process of (2S,3S)-2-tert-Butoxycarbonylamino-3-(tert-butyl-dimethyl-silanyloxy)-succinic acid 4-benzyl ester

There total 6 articles about (2S,3S)-2-tert-Butoxycarbonylamino-3-(tert-butyl-dimethyl-silanyloxy)-succinic acid 4-benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: (2S,3S)-2-tert-Butoxycarbonylamino-3-hydroxy-succinic acid 4-benzyl ester

: 207510-42-7
(2S,3S)-2-tert-Butoxycarbonylamino-3-(tert-butyl-dimethyl-silanyloxy)-succinic acid 4-benzyl ester

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; Yield given;
DOI:10.1021/ja00134a035

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 207510-42-7
(2S,3S)-2-tert-Butoxycarbonylamino-3-(tert-butyl-dimethyl-silanyloxy)-succinic acid 4-benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: TEA / dioxane; H₂O

2: imidazole / dimethylformamide

With 1H-imidazole; TEA; In 1,4-dioxane; water; N,N-dimethyl-formamide;
DOI:10.1021/ja00134a035

Reference yield:

: 19516-01-9
(2S,3S)-2-amino-4-(benzyloxy)-3-hydroxy-4-oxobutanoic acid

: 207510-42-7
(2S,3S)-2-tert-Butoxycarbonylamino-3-(tert-butyl-dimethyl-silanyloxy)-succinic acid 4-benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: TEA / dioxane; H₂O

2: imidazole / dimethylformamide

With 1H-imidazole; TEA; In 1,4-dioxane; water; N,N-dimethyl-formamide;
DOI:10.1021/ja00134a035