(S)-2-{N-benzyl-N-[(1-n-butylpyrrolidin-2-yl)methyl]aminomethyl}-4-methyl-6-(triphenylmethyl)phenol

Base Information

Chemical Name:(S)-2-{N-benzyl-N-[(1-n-butylpyrrolidin-2-yl)methyl]aminomethyl}-4-methyl-6-(triphenylmethyl)phenol
CAS No.:1454866-50-2
Molecular Formula:C₄₃H₄₈N₂O
Molecular Weight:608.867
Hs Code.:

Synonyms:(S)-2-{N-benzyl-N-[(1-n-butylpyrrolidin-2-yl)methyl]aminomethyl}-4-methyl-6-(triphenylmethyl)phenol

Suppliers and Price of (S)-2-{N-benzyl-N-[(1-n-butylpyrrolidin-2-yl)methyl]aminomethyl}-4-methyl-6-(triphenylmethyl)phenol

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Chemical Property of (S)-2-{N-benzyl-N-[(1-n-butylpyrrolidin-2-yl)methyl]aminomethyl}-4-methyl-6-(triphenylmethyl)phenol

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Technology Process of (S)-2-{N-benzyl-N-[(1-n-butylpyrrolidin-2-yl)methyl]aminomethyl}-4-methyl-6-(triphenylmethyl)phenol

There total 5 articles about (S)-2-{N-benzyl-N-[(1-n-butylpyrrolidin-2-yl)methyl]aminomethyl}-4-methyl-6-(triphenylmethyl)phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.8%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 223706-42-1
4-methyl-2-tritylphenol

: 130981-38-3
(S)-(1-ⁿbutylpyrrolidin-2-yl)methanamine

: 100-52-7
benzaldehyde

: 1454866-50-2
(S)-2-{N-benzyl-N-[(1-n-butylpyrrolidin-2-yl)methyl]aminomethyl}-4-methyl-6-(triphenylmethyl)phenol

Guidance literature:: (S)-(1-ⁿbutylpyrrolidin-2-yl)methanamine; benzaldehyde; In ethanol; for 24h; Reflux;

With sodium tetrahydroborate; In ethanol; for 3h;

formaldehyd; 4-methyl-2-tritylphenol; In ethanol; for 12h; Reflux;

Reference yield: 89.8%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 1454866-39-7
(S)-N-benzyl-1-(1-ⁿbutylpyrrolidin-2-yl)methanamine

: 223706-42-1
4-methyl-2-tritylphenol

: 1454866-50-2
(S)-2-{N-benzyl-N-[(1-n-butylpyrrolidin-2-yl)methyl]aminomethyl}-4-methyl-6-(triphenylmethyl)phenol

Guidance literature:: In ethanol; at 90 ℃; for 12h; Inert atmosphere;
DOI:10.1039/c3cc44980g

Reference yield:

: 130981-38-3
(S)-(1-ⁿbutylpyrrolidin-2-yl)methanamine

: 1454866-50-2
(S)-2-{N-benzyl-N-[(1-n-butylpyrrolidin-2-yl)methyl]aminomethyl}-4-methyl-6-(triphenylmethyl)phenol

Guidance literature:: Multi-step reaction with 3 steps

1: ethanol / 24 h / Inert atmosphere; Reflux

2: sodium tetrahydroborate / ethanol / 3 h / 60 °C / Inert atmosphere

3: ethanol / 12 h / 90 °C / Inert atmosphere

With sodium tetrahydroborate; In ethanol;
DOI:10.1039/c3cc44980g