(1R,2S,3R,4S)-3,4-Bis-(3-methoxy-phenyl)-cyclobutane-1,2-dicarboxylic acid dimethyl ester

Base Information Edit

Chemical Name:(1R,2S,3R,4S)-3,4-Bis-(3-methoxy-phenyl)-cyclobutane-1,2-dicarboxylic acid dimethyl ester
CAS No.:141396-24-9
Molecular Formula:C₂₂H₂₄O₆
Molecular Weight:384.429
Hs Code.:
Mol file:141396-24-9.mol

Synonyms:(1R,2S,3R,4S)-3,4-Bis-(3-methoxy-phenyl)-cyclobutane-1,2-dicarboxylic acid dimethyl ester

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Chemical Property of (1R,2S,3R,4S)-3,4-Bis-(3-methoxy-phenyl)-cyclobutane-1,2-dicarboxylic acid dimethyl ester Edit

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Technology Process of (1R,2S,3R,4S)-3,4-Bis-(3-methoxy-phenyl)-cyclobutane-1,2-dicarboxylic acid dimethyl ester

There total 5 articles about (1R,2S,3R,4S)-3,4-Bis-(3-methoxy-phenyl)-cyclobutane-1,2-dicarboxylic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 15854-56-5
3-methoxy-cinnamic acid methyl ester

: 141396-24-9
(1R,2S,3R,4S)-3,4-Bis-(3-methoxy-phenyl)-cyclobutane-1,2-dicarboxylic acid dimethyl ester

: dimethyl t-3,c-4-di-(3-methoxyphenyl)cyclobutane-r-1,t-2-dicarboxylate

Guidance literature:: In acetonitrile; for 30h; Product distribution; Irradiation; other substituted cinnamic acid methyl ester; with or without benzophenon as sensitizer;
DOI:10.1016/S0040-4020(01)88772-X

Reference yield:

: 6099-04-3,17570-26-2
trans-3-methoxycinnamic acid

: 141396-24-9
(1R,2S,3R,4S)-3,4-Bis-(3-methoxy-phenyl)-cyclobutane-1,2-dicarboxylic acid dimethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: p-toluene sulfonic acid / 12 h / Heating

2: tris(4-pyridyl)1,3,5-triazine-based Pd(II) complex / D₂O / 3 h / Irradiation

With toluene-4-sulfonic acid; tris(4-pyridyl)1,3,5-triazine-based Pd(II); In water-d2;
DOI:10.1021/jo0617722