N-(4-Methanesulfonylamino-phenyl)-2-(2-methyl-propane-2-sulfinyl)-nicotinamide

Base Information

Chemical Name:N-(4-Methanesulfonylamino-phenyl)-2-(2-methyl-propane-2-sulfinyl)-nicotinamide
CAS No.:1027411-17-1
Molecular Formula:C₁₇H₂₁N₃O₄S₂
Molecular Weight:395.503
Hs Code.:

Synonyms:N-(4-Methanesulfonylamino-phenyl)-2-(2-methyl-propane-2-sulfinyl)-nicotinamide

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Chemical Property of N-(4-Methanesulfonylamino-phenyl)-2-(2-methyl-propane-2-sulfinyl)-nicotinamide

Chemical Property:

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Technology Process of N-(4-Methanesulfonylamino-phenyl)-2-(2-methyl-propane-2-sulfinyl)-nicotinamide

There total 4 articles about N-(4-Methanesulfonylamino-phenyl)-2-(2-methyl-propane-2-sulfinyl)-nicotinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1026900-83-3
2-tert-Butylsulfanyl-N-(4-methanesulfonylamino-phenyl)-nicotinamide

: 1027411-17-1
N-(4-Methanesulfonylamino-phenyl)-2-(2-methyl-propane-2-sulfinyl)-nicotinamide

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In chloroform;
DOI:10.1021/jm00045a012

Reference yield:

: 49609-84-9
2-Chloronicotinoyl chloride

: 1027411-17-1
N-(4-Methanesulfonylamino-phenyl)-2-(2-methyl-propane-2-sulfinyl)-nicotinamide

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine, DMF / CH₂Cl₂ / 1.5 h / 0 °C

2: KOtBu / 2-methyl-propan-2-ol / 2 h / Heating

3: m-CPBA / CHCl₃

With pyridine; potassium tert-butylate; N,N-dimethyl-formamide; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; chloroform; tert-butyl alcohol;
DOI:10.1021/jm00045a012

Reference yield:

: 2942-59-8
2-chloronicotinic acid

: 1027411-17-1
N-(4-Methanesulfonylamino-phenyl)-2-(2-methyl-propane-2-sulfinyl)-nicotinamide

Guidance literature:: Multi-step reaction with 4 steps

1: oxalyl chloride, DMF / CH₂Cl₂ / 0.67 h / Heating

2: pyridine, DMF / CH₂Cl₂ / 1.5 h / 0 °C

3: KOtBu / 2-methyl-propan-2-ol / 2 h / Heating

4: m-CPBA / CHCl₃

With pyridine; oxalyl dichloride; potassium tert-butylate; N,N-dimethyl-formamide; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; chloroform; tert-butyl alcohol;
DOI:10.1021/jm00045a012