{[(3S)-3-(4-{[(1R)-4,6-Dimethyl-2,3-dihydro-1H-inden-1-yl]oxy}phenyl)-3-ethoxypropyl]oxy}(triisopropyl)silane

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Chemical Name:{[(3S)-3-(4-{[(1R)-4,6-Dimethyl-2,3-dihydro-1H-inden-1-yl]oxy}phenyl)-3-ethoxypropyl]oxy}(triisopropyl)silane
CAS No.:1202578-17-3
Molecular Formula:C₃₁H₄₈O₃Si
Molecular Weight:496.806
Hs Code.:

Synonyms:{[(3S)-3-(4-{[(1R)-4,6-Dimethyl-2,3-dihydro-1H-inden-1-yl]oxy}phenyl)-3-ethoxypropyl]oxy}(triisopropyl)silane

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Chemical Property of {[(3S)-3-(4-{[(1R)-4,6-Dimethyl-2,3-dihydro-1H-inden-1-yl]oxy}phenyl)-3-ethoxypropyl]oxy}(triisopropyl)silane

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Technology Process of {[(3S)-3-(4-{[(1R)-4,6-Dimethyl-2,3-dihydro-1H-inden-1-yl]oxy}phenyl)-3-ethoxypropyl]oxy}(triisopropyl)silane

There total 10 articles about {[(3S)-3-(4-{[(1R)-4,6-Dimethyl-2,3-dihydro-1H-inden-1-yl]oxy}phenyl)-3-ethoxypropyl]oxy}(triisopropyl)silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 1202577-78-3
4-{(1S)-1-ethoxy-3-[(triisopropylsilyl)oxy]propyl}phenol

: 1202578-16-2
(1S)-4,6-dimethylindan-1-ol

: 1202578-17-3
{[(3S)-3-(4-{[(1R)-4,6-Dimethyl-2,3-dihydro-1H-inden-1-yl]oxy}phenyl)-3-ethoxypropyl]oxy}(triisopropyl)silane

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; toleuene; at 20 ℃; Inert atmosphere;

Reference yield:

: 15764-16-6
2,4-dimethylbenzaldehyde

: 1202578-17-3
{[(3S)-3-(4-{[(1R)-4,6-Dimethyl-2,3-dihydro-1H-inden-1-yl]oxy}phenyl)-3-ethoxypropyl]oxy}(triisopropyl)silane

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / tetrahydrofuran / 0 °C / Inert atmosphere

1.2: 0 °C / Inert atmosphere

2.1: hydrogen / ethanol / 20 °C

2.2: 20 °C

3.1: polyphosphoric acid / water / 1 h / 90 °C / Cooling with ice

4.1: triethylamine; formic acid / Noyori's catalyst / dichloromethane / 20 - 40 °C / Inert atmosphere

5.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran; toleuene / 20 °C / Inert atmosphere

With formic acid; hydrogen; sodium hydride; triethylamine; triphenylphosphine; diethylazodicarboxylate; Noyori's catalyst; In tetrahydrofuran; ethanol; dichloromethane; toleuene; water;

Reference yield:

: 1811-85-4
3-(2,4-dimethylphenyl)propionic acid

: 1202578-17-3
{[(3S)-3-(4-{[(1R)-4,6-Dimethyl-2,3-dihydro-1H-inden-1-yl]oxy}phenyl)-3-ethoxypropyl]oxy}(triisopropyl)silane

Guidance literature:: Multi-step reaction with 3 steps

1: polyphosphoric acid / water / 1 h / 90 °C / Cooling with ice

2: triethylamine; formic acid / Noyori's catalyst / dichloromethane / 20 - 40 °C / Inert atmosphere

3: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran; toleuene / 20 °C / Inert atmosphere

With formic acid; triethylamine; triphenylphosphine; diethylazodicarboxylate; Noyori's catalyst; In tetrahydrofuran; dichloromethane; toleuene; water;