Methanesulfonic acid (3E,7E,11E)-3,7,11-trimethyl-1-[2-methyl-1-(tetrahydro-pyran-2-yloxy)-propyl]-13-phenylsulfanyl-trideca-3,7,11-trienyl ester

Base Information

Chemical Name:Methanesulfonic acid (3E,7E,11E)-3,7,11-trimethyl-1-[2-methyl-1-(tetrahydro-pyran-2-yloxy)-propyl]-13-phenylsulfanyl-trideca-3,7,11-trienyl ester
CAS No.:125458-58-4
Molecular Formula:C₃₂H₅₀O₅S₂
Molecular Weight:578.878
Hs Code.:

Methanesulfonic acid (3E,7E,11E)-3,7,11-trimethyl-1-[2-methyl-1-(tetrahydro-pyran-2-yloxy)-propyl]-13-phenylsulfanyl-trideca-3,7,11-trienyl ester

Synonyms:Methanesulfonic acid (3E,7E,11E)-3,7,11-trimethyl-1-[2-methyl-1-(tetrahydro-pyran-2-yloxy)-propyl]-13-phenylsulfanyl-trideca-3,7,11-trienyl ester

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Chemical Property of Methanesulfonic acid (3E,7E,11E)-3,7,11-trimethyl-1-[2-methyl-1-(tetrahydro-pyran-2-yloxy)-propyl]-13-phenylsulfanyl-trideca-3,7,11-trienyl ester

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Technology Process of Methanesulfonic acid (3E,7E,11E)-3,7,11-trimethyl-1-[2-methyl-1-(tetrahydro-pyran-2-yloxy)-propyl]-13-phenylsulfanyl-trideca-3,7,11-trienyl ester

There total 9 articles about Methanesulfonic acid (3E,7E,11E)-3,7,11-trimethyl-1-[2-methyl-1-(tetrahydro-pyran-2-yloxy)-propyl]-13-phenylsulfanyl-trideca-3,7,11-trienyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 124-63-0
methanesulfonyl chloride

: 125458-53-9
(6E,10E,14E)-2,6,10,14-tetramethyl-16-phenylthio-3-tetrahydropyranyloxy-6,10,14-hexadecatrien-4-ol

: 125458-58-4
Methanesulfonic acid (3E,7E,11E)-3,7,11-trimethyl-1-[2-methyl-1-(tetrahydro-pyran-2-yloxy)-propyl]-13-phenylsulfanyl-trideca-3,7,11-trienyl ester

Guidance literature:: With pyridine; at 0 ℃; for 4h;

Reference yield:

: 110-87-2
3,4-dihydro-2H-pyran

: 125458-58-4
Methanesulfonic acid (3E,7E,11E)-3,7,11-trimethyl-1-[2-methyl-1-(tetrahydro-pyran-2-yloxy)-propyl]-13-phenylsulfanyl-trideca-3,7,11-trienyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / p-TsOH / CH₂Cl₂ / 4 h / Ambient temperature

2: 94 percent / 2N NaOH / methanol / 24 h / Heating

3: 96 percent / pyridine / 4 h / 0 °C

With pyridine; sodium hydroxide; toluene-4-sulfonic acid; In methanol; dichloromethane;

Reference yield:

: 31236-13-2,60441-27-2,69538-05-2,69538-06-3,69659-77-4,69659-78-5,74986-29-1
10,11-oxido-E,E-farnesyl phenyl sulfide

: 125458-58-4
Methanesulfonic acid (3E,7E,11E)-3,7,11-trimethyl-1-[2-methyl-1-(tetrahydro-pyran-2-yloxy)-propyl]-13-phenylsulfanyl-trideca-3,7,11-trienyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 82 percent / aluminium isopropoxide / toluene / 12 h / Heating

2: 60 percent / 2,4-dinitrophenol / toluene / 1) heated gradually to 125 deg C over 3 h, 2) 125 deg C, 30 h

3: 100 percent / NaBH₄ / methanol / 0.5 h / Ambient temperature

4: 95 percent / p-TsOH / CH₂Cl₂ / 4 h / Ambient temperature

5: 94 percent / 2N NaOH / methanol / 24 h / Heating

6: 96 percent / pyridine / 4 h / 0 °C

With pyridine; sodium hydroxide; sodium tetrahydroborate; 2,4-Dinitrophenol; aluminum isopropoxide; toluene-4-sulfonic acid; In methanol; dichloromethane; toluene;