N-(1-benzyl-4-piperidinyl)-2-methoxy-5-(N-(4-toluenesulfonyl)amino)benzamide

Base Information

Chemical Name:N-(1-benzyl-4-piperidinyl)-2-methoxy-5-(N-(4-toluenesulfonyl)amino)benzamide
CAS No.:130259-97-1
Molecular Formula:C₂₇H₃₁N₃O₄S
Molecular Weight:493.627
Hs Code.:

Synonyms:N-(1-benzyl-4-piperidinyl)-2-methoxy-5-(N-(4-toluenesulfonyl)amino)benzamide

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Chemical Property of N-(1-benzyl-4-piperidinyl)-2-methoxy-5-(N-(4-toluenesulfonyl)amino)benzamide

Chemical Property:

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Technology Process of N-(1-benzyl-4-piperidinyl)-2-methoxy-5-(N-(4-toluenesulfonyl)amino)benzamide

There total 6 articles about N-(1-benzyl-4-piperidinyl)-2-methoxy-5-(N-(4-toluenesulfonyl)amino)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 130259-93-7
N-(1-benzyl-4-piperidinyl)-5-amino-2-methoxybenzamide

: 98-59-9
p-toluenesulfonyl chloride

: 130259-97-1
N-(1-benzyl-4-piperidinyl)-2-methoxy-5-(N-(4-toluenesulfonyl)amino)benzamide

Guidance literature:: With sodium hydrogencarbonate; In dichloromethane; for 3h; Ambient temperature;

Reference yield:

: 3612-20-2
1-phenylmethyl-4-piperidone

: 130259-97-1
N-(1-benzyl-4-piperidinyl)-2-methoxy-5-(N-(4-toluenesulfonyl)amino)benzamide

Guidance literature:: Multi-step reaction with 5 steps

1: formic acid / 1.) 100 - 125 deg C, 30 min, 2.) 170 deg C, 5 h

2: 97 percent / KOH / ethanol / 4 h / Heating

3: 100 percent / CHCl₃ / 1.5 h / Heating

4: 76 percent / N₂H₄*H₂O, Raney Ni / ethanol / 1.5 h / 60 °C

5: 96 percent / NaHCO₃ / CH₂Cl₂ / 3 h / Ambient temperature

With potassium hydroxide; formic acid; nickel; sodium hydrogencarbonate; hydrazine hydrate; In ethanol; dichloromethane; chloroform;

Reference yield:

: 50541-93-0
4-amino-1-benzylpiperidine

: 130259-97-1
N-(1-benzyl-4-piperidinyl)-2-methoxy-5-(N-(4-toluenesulfonyl)amino)benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / CHCl₃ / 1.5 h / Heating

2: 76 percent / N₂H₄*H₂O, Raney Ni / ethanol / 1.5 h / 60 °C

3: 96 percent / NaHCO₃ / CH₂Cl₂ / 3 h / Ambient temperature

With nickel; sodium hydrogencarbonate; hydrazine hydrate; In ethanol; dichloromethane; chloroform;