[(1S,2S)-2-((R)-1-Ethoxymethoxy-2,2-dimethyl-propyl)-cyclohexyl]-diethyl-borane

Base Information

• Chemical Name: [(1S,2S)-2-((R)-1-Ethoxymethoxy-2,2-dimethyl-propyl)-cyclohexyl]-diethyl-borane
• CAS No.: 289488-82-0
• Molecular Formula: C₁₈H₃₇BO₂
• Molecular Weight: 296.302

Synonyms:[(1S,2S)-2-((R)-1-Ethoxymethoxy-2,2-dimethyl-propyl)-cyclohexyl]-diethyl-borane

Chemical Property of [(1S,2S)-2-((R)-1-Ethoxymethoxy-2,2-dimethyl-propyl)-cyclohexyl]-diethyl-borane

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Technology Process of [(1S,2S)-2-((R)-1-Ethoxymethoxy-2,2-dimethyl-propyl)-cyclohexyl]-diethyl-borane

There total 1 articles about [(1S,2S)-2-((R)-1-Ethoxymethoxy-2,2-dimethyl-propyl)-cyclohexyl]-diethyl-borane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Diethylborane (5518-25-2) + 1-(1-ethoxymethoxy-2,2-dimethyl-propyl)-cyclohexene → [(1S,2S)-2-((R)-1-Ethoxymethoxy-2,2-dimethyl-propyl)-cyclohexyl]-diethyl-borane (289488-82-0)

Guidance literature:

With dimethylsulfide; at 50 ℃; for 16h; Title compound not separated from byproducts;

DOI:10.1002/1521-3773(20000703)39:13<2294::AID-ANIE2294>3.0.CO;2-J

Reference yield:

propionyl chloride (79-03-8) + [(1S,2S)-2-((R)-1-Ethoxymethoxy-2,2-dimethyl-propyl)-cyclohexyl]-diethyl-borane (289488-82-0) → 1-[(1R,2R)-2-((S)-1-Ethoxymethoxy-2,2-dimethyl-propyl)-cyclohexyl]-propan-1-one

Guidance literature:

[(1S,2S)-2-((R)-1-Ethoxymethoxy-2,2-dimethyl-propyl)-cyclohexyl]-diethyl-borane; With diisopropyl zinc; In diethyl ether; at 25 ℃; for 5h;

In tetrahydrofuran; at -78 ℃; for 0.5h;

propionyl chloride; In tetrahydrofuran; at -78 - 25 ℃; for 12h;

DOI:10.1002/1521-3773(20000703)39:13<2294::AID-ANIE2294>3.0.CO;2-J

Reference yield:

allyl bromide (106-95-6) + [(1S,2S)-2-((R)-1-Ethoxymethoxy-2,2-dimethyl-propyl)-cyclohexyl]-diethyl-borane (289488-82-0) → (1S,2R)-1-Allyl-2-((S)-1-ethoxymethoxy-2,2-dimethyl-propyl)-cyclohexane

Guidance literature:

[(1S,2S)-2-((R)-1-Ethoxymethoxy-2,2-dimethyl-propyl)-cyclohexyl]-diethyl-borane; With diisopropyl zinc; In diethyl ether; at 25 ℃; for 5h;

In tetrahydrofuran; at -78 ℃; for 0.5h;

allyl bromide; In tetrahydrofuran; at -78 - 25 ℃; for 12h;

DOI:10.1002/1521-3773(20000703)39:13<2294::AID-ANIE2294>3.0.CO;2-J

upstream raw materials:

Diethylborane

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